SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES

SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES

Hematite nanoparticles were prepared by a procedure consisting in sonication of μ3-oxo trinuclear iron(III) acetate of composition [Fe3O(OOCCH3)6(H2O)3]NO3∙4H2O, {Fe3O}NO3 as iron source, in strong basic conditions followed by thermal treatment at 600˚C. The formation of the hematite was confirmed b...

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Main Author: Mihail Iacob
Format: Article
Language:English
Published: Academy of Sciences of Moldova, Institute of Chemistry 2015-06-01
Series:Chemistry Journal of Moldova: General, Industrial and Ecological Chemistry
Subjects:
hematite
nanoparticles
iron oxides
sonochemistry
Online Access:http://www.cjm.asm.md/sites/default/files/article_files/ChemJMold201510(1)_46-51_Iacob.pdf
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spelling doaj-707f5ee8d1964afa86c632a0e54001722021-07-02T13:37:45ZengAcademy of Sciences of Moldova, Institute of ChemistryChemistry Journal of Moldova: General, Industrial and Ecological Chemistry1857-17272345-16882015-06-011014651SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLESMihail Iacob 0“Petru Poni” Institute of Macromolecular Chemistry, Institute of Chemistry of the Academy of Sciences of Moldova, Hematite nanoparticles were prepared by a procedure consisting in sonication of μ3-oxo trinuclear iron(III) acetate of composition [Fe3O(OOCCH3)6(H2O)3]NO3∙4H2O, {Fe3O}NO3 as iron source, in strong basic conditions followed by thermal treatment at 600˚C. The formation of the hematite was confirmed by IR spectroscopy, X-ray powder diffraction and Raman spectroscopy while the shape and size of the nanoparticles and their agglomeration were evidenced and estimated on the basis of the images taken with TEM techniques. http://www.cjm.asm.md/sites/default/files/article_files/ChemJMold201510(1)_46-51_Iacob.pdfhematitenanoparticlesiron oxidessonochemistry
collection DOAJ
language English
format Article
sources DOAJ
author Mihail Iacob
spellingShingle Mihail Iacob
SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES
Chemistry Journal of Moldova: General, Industrial and Ecological Chemistry
hematite
nanoparticles
iron oxides
sonochemistry
author_facet Mihail Iacob
author_sort Mihail Iacob
title SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES
title_short SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES
title_full SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES
title_fullStr SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES
title_full_unstemmed SONOCHEMICAL SYNTHESIS OF HEMATITE NANOPARTICLES
title_sort sonochemical synthesis of hematite nanoparticles
publisher Academy of Sciences of Moldova, Institute of Chemistry
series Chemistry Journal of Moldova: General, Industrial and Ecological Chemistry
issn 1857-1727
2345-1688
publishDate 2015-06-01
description Hematite nanoparticles were prepared by a procedure consisting in sonication of μ3-oxo trinuclear iron(III) acetate of composition [Fe3O(OOCCH3)6(H2O)3]NO3∙4H2O, {Fe3O}NO3 as iron source, in strong basic conditions followed by thermal treatment at 600˚C. The formation of the hematite was confirmed by IR spectroscopy, X-ray powder diffraction and Raman spectroscopy while the shape and size of the nanoparticles and their agglomeration were evidenced and estimated on the basis of the images taken with TEM techniques.
topic hematite
nanoparticles
iron oxides
sonochemistry
url http://www.cjm.asm.md/sites/default/files/article_files/ChemJMold201510(1)_46-51_Iacob.pdf
work_keys_str_mv AT mihailiacob sonochemicalsynthesisofhematitenanoparticles
_version_ 1721328876207996928

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