Determination of glyphosate and its derivative, aminomethylphosphonic acid, in human urine by gas chromatography coupled to tandem mass spectrometry and isotope pattern deconvolution

An analytical method for the simultaneous determination of glyphosate (GLY) and its main derivative, aminomethyl-phosphonic acid (AMPA), in human urine has been developed using gas chromatography coupled to tandem mass spectrometry (MS/MS) operated in multiple reaction monitoring mode (MRM). Sample...

Full description

Bibliographic Details
Published in:	Journal of Chromatography Open
Main Authors:	Eva Junqué, Pilar Fernández, Iohanna Filippi, Joan O. Grimalt
Format:	Article
Language:	English
Published:	Elsevier 2023-11-01
Subjects:	Polar pesticides Isotope dilution Biomonitoring Gas chromatography Tandem mass spectrometry in negative ion chemical ionization
Online Access:	http://www.sciencedirect.com/science/article/pii/S2772391723000117

Similar Items

Determination of 12 pesticide metabolites in human urine by liquid chromatography-tandem mass spectrometry
by: Yujie CHEN, et al.
Published: (2024-08-01)

Determination of Pentachlorophenol in Milk Powder by Isotope Dilution Liquid Chromatography-Tandem Mass Spectrometry
by: QI Yan, LI Jinqing, LI Cong, XU Qingpeng
Published: (2023-08-01)

Occurrence and profiles of glyphosate and aminomethylphosphonic acid in paired urine and feces of humans, cats, and dogs
by: Zhong-Min Li, et al.
Published: (2025-05-01)

Validation of a Liquid Chromatography Coupled to Mass Spectrometry Method for Glyphosate and Aminomethylphosphonic Acid in Urine for Human Biomonitoring Using Combined Hybrid Anion-Exchange and Hydrophilic Interaction Liquid Chromatography
by: Elisa Polledri, et al.
Published: (2023-11-01)

Determination of 3-Methoxytyramine and Adrenaline in Dairy Products by Isotopic Dilution-Assisted Liquid Chromatography-Tandem Mass Spectrometry
by: Yanmei BAI, et al.
Published: (2023-10-01)

Determination of Residues of 5-Nitroimidazoles and Their Metabolites in Eggs by Isotope Dilution-Ultra-high Performance Liquid Chromatography-Tandem Mass Spectrometry
by: QIU Xiaoyi, WANG Dongmei, LI Jiakuan, XU Qing, WANG Mengying, GUAN Zhuolong, LU Yuepeng, TU Fengqin
Published: (2023-11-01)

Isotope dilution-ultra performance liquid chromatography-tandem mass spectrometry for determination of five alternariol mycotoxins in chestnut
by: Quanshuai WANG, et al.
Published: (2025-06-01)

Candidate reference measurement procedure for serum 17‐hydroxyprogesterone quantification via isotope dilution liquid chromatography–tandem mass spectrometry
by: Ji Zhang, et al.
Published: (2024-06-01)

Fast and Sensitive Analysis of Cefiderocol in Human Plasma Microsamples by Liquid Chromatography-Isotope Dilution Tandem Mass Spectrometry for Therapeutic Drug Monitoring
by: Rossella Barone, et al.
Published: (2023-01-01)

Fast and Simple Liquid Chromatography-Isotope Dilution Tandem Mass Spectrometry Method for Therapeutic Drug Monitoring of Dalbavancin in Long-Term Treatment of Subacute and/or Chronic Infections
by: Rossella Barone, et al.
Published: (2023-02-01)

Determination of glyphosate and aminomethylphosphonic acid residues in Finnish soils by ultra‐high performance liquid chromatography–tandem mass spectrometry
by: Sari Rämö, et al.
Published: (2023-12-01)

Development of an isotope dilution liquid chromatography/tandem mass spectrometry method for the accurate determination of neonicotinoid pesticides, imidacloprid, clothianidin, and thiamethoxam in kimchi cabbage reference materials
by: Seonghee Ahn, et al.
Published: (2022-03-01)

Development of isotope dilution-liquid chromatography tandem mass spectrometry for the accurate determination of vitamin K1 in spinach and kimchi cabbage
by: Hyeyoung Lee, et al.
Published: (2023-09-01)

Occurrence of Pesticide Residues in Spanish Honey Measured by QuEChERS Method Followed by Liquid and Gas Chromatography–Tandem Mass Spectrometry
by: Roberto Jesús Lasheras, et al.
Published: (2021-09-01)

Non-Invasive Monitoring of Corticosterone Levels in Mouse Urine with Liquid Chromatography-Electrospray Ionization-Tandem Mass Spectrometry
by: Laura Howe-Wittek, et al.
Published: (2024-11-01)

Validation and Application of Liquid Chromatography Coupled with Tandem Mass Spectrometry Method for the Analysis of Glyphosate, Aminomethylphosphonic Acid (AMPA), and Glufosinate in Soil
by: José Belisario Leyva-Morales, et al.
Published: (2023-05-01)

Unveiling the Impacts of Glyphosate, Deltamethrin, Propamocarb and Tebuconazole on Gut Health
by: Kimberly Fenech, et al.
Published: (2025-09-01)

A review on advances and perspectives of glyphosate determination: challenges and opportunities
by: Kumsal Kocadal, et al.
Published: (2022-09-01)

Simultaneous determination of 375 pesticide residues in milk by high performance liquid chromatography-tandem mass spectrometry
by: ZHANG Lijia, BAI Yanmei, WANG Yang, LIU Lijun, XIE Ruilong, MO Nan, GAO Yujie, LI Peizhen, LI Cuizhi
Published: (2024-05-01)

Determination of 14 Pesticide Residues in Tea by QuEChERS Combined with Ultra-performance Liquid Chromatography-tandem Mass Spectrometry
by: Yingjie ZHU, et al.
Published: (2022-06-01)

Determination of Parabens, Bisphenol A and Its Analogs, Triclosan, and Benzophenone-3 Levels in Human Urine by Isotope-Dilution-UPLC-MS/MS Method Followed by Supported Liquid Extraction
by: Hsin-Chang Chen, et al.
Published: (2022-01-01)

Detection of glyphosate and its metabolite aminomethylphosphonic acid: Risk assessment for the aquatic organisms
by: Nikola Puvača, et al.
Published: (2024-06-01)

Simultaneous determination of 15 pesticide residues in Chinese cabbage and cucumber by liquid chromatography-tandem mass spectrometry utilizing online turbulent flow chromatography
by: Sufang Fan, et al.
Published: (2021-01-01)

Relationship between Urine Creatinine and Urine Osmolality in Spot Samples among Men and Women in the Danish Diet Cancer and Health Cohort
by: Selinay Ozdemir, et al.
Published: (2021-11-01)

Determination of 20 Pesticide Residues in Cosmetic Containing Plant Extracts by Liquid Chromatography Tandem Mass Spectrometry
by: YANG Jin-qing, et al.
Published: (2021-11-01)

A paper-based device for glyphosate electrochemical detection in human urine: A case study to demonstrate how the properties of the paper can solve analytical issues
by: Giulia Moro, et al.
Published: (2023-12-01)

Analytical method for the biomonitoring of bisphenols and parabens by liquid chromatography coupled to tandem mass spectrometry in human hair
by: Julien Robin, et al.
Published: (2022-09-01)

Supramolecular Solvent Extraction-Gas Chromatography-Tandem Mass Spectrometry for Detection of Benzodiazepines in Urines
by: LIU Jin-lei, GU Jie, CHEN Li-qin, et al.
Published: (2021-02-01)

Multiresidual gas chromatography-tandem mass spectrometry method for determination of plant protection product residues in fruit
by: Helena BAŠA ČESNIK
Published: (2025-06-01)

Simultaneous toxicokinetics characterization of acrylamide and its primary metabolites using a novel microdialysis isotope-dilution liquid chromatography mass spectrometry method
by: Yu-Syuan Luo, et al.
Published: (2022-01-01)

Glyphosate and AMPA in saliva and other traditional human matrices. New findings for less invasive biomonitoring to the exposure to pesticides
by: Iohanna Filippi, et al.
Published: (2024-04-01)

Determination of Eight Amide Herbicide Residues in Animal-derived Foods by Gas Chromatography-Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry
by: YANG Zhijin, LIN Binbin, HUANG Xuliang, CHEN Qianni, LIN Xiaolian, LAN Yanshan
Published: (2023-11-01)

Rapid Determination of Tetracyclines in Drinking and Environmental Waters Using Fully Automatic Solid-Phase Extraction with Ultra-Performance Liquid Chromatography–Tandem Mass Spectrometry
by: Tongtong Zhang, et al.
Published: (2024-06-01)

Determination of glufosinate ammonium and three metabolites in urine by ultra performance liquid chromatography-tandem mass spectrometry
by: Yingru LING, et al.
Published: (2024-06-01)

Determination of Residual Behavior of Flufenacet in Wheat and its Dietary Risk Assessment by Liquid Chromatography-Tandem Mass Spectrometry
by: Jing YANG, et al.
Published: (2025-05-01)

Determination of 24 pesticide residues in fresh edible fungiby dispersive solid phase extraction-gas chromatography coupled with tandem mass spectrometry
by: SHEN Xia
Published: (2023-04-01)

Determination of veterinary drug residues, mycotoxins, and pesticide residues in bovine milk by liquid chromatography electrospray ionisation –tandem mass spectrometry
by: Hajrulai-Musliu Zehra, et al.
Published: (2022-05-01)

Determination of <i>Alternaria</i> Toxins in Sunflower Oil by Liquid Chromatography Isotope Dilution Tandem Mass Spectrometry
by: Ádám Tölgyesi, et al.
Published: (2020-04-01)

Characterization and Determination of the Alkaloid Metabolites of Evodiae fructus in Rat Urine by Liquid Chromatography-Tandem Mass Spectrometry Detection
by: Youping Liu, et al.
Published: (2011-07-01)

Effect of fermentation stages on glucosinolate profiles in kimchi: Quantification of 14 intact glucosinolates using ultra-performance liquid chromatography-tandem mass spectrometry
by: Su-Yeon Kim, et al.
Published: (2022-10-01)