| Summary: | Semiconductor-based photocatalyst materials played an important role in the degradation of organic compounds in recent years. Photocatalysis is a simple, cost-effective, and environmentally friendly process for degrading organic compounds. In this work, vanadium pentoxide (V<sub>2</sub>O<sub>5</sub>) and V<sub>2</sub>O<sub>5</sub>/RGO (reduced graphene oxide) composite were synthesized by a hydrothermal method. The prepared samples were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), Raman spectroscopy, and UV-Vis spectroscopic analysis, etc. Raman analysis shows the occurrence of RGO characteristic peaks in the composite and different vibrational modes of V<sub>2</sub>O<sub>5</sub>. The band gap of flake-shaped V<sub>2</sub>O<sub>5</sub> is reduced and its light absorption capacity is enhanced by making its composite with RGO. The photocatalytic degradation of methylene blue (MB) was studied using both V<sub>2</sub>O<sub>5</sub> and V<sub>2</sub>O<sub>5</sub>/RGO composite photocatalyst materials. The V<sub>2</sub>O<sub>5</sub>/RGO composite exhibits a superior photocatalytic performance to V<sub>2</sub>O<sub>5</sub>. Both catalyst and light play an important role in the degradation process.
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