| Summary: | 邻苯二甲酸酯（PAEs）类塑化剂是一种环境污染物，具有生殖毒性，易致癌、致畸，植物油易受到PAEs污染。旨在为植物油中PAEs类塑化剂检测方法的开发提供参考，对植物油中PAEs类塑化剂检测技术的前处理方法和定量检测技术进行了综述，比较了各方法的优缺点，并对其发展趋势进行了展望。PAEs类塑化剂检测的前处理方法包括液-液萃取法、固相萃取法、凝胶渗透色谱法和QuEChERS法等；定量检测技术包括高效液相色谱法、气相色谱法、液相色谱-质谱联用法、气相色谱-质谱联用法等。未来联合前处理技术、在线净化、微萃取，以及三重四极杆气相色谱-质谱联用技术等将成为PAEs类塑化剂检测的发展方向。
Phthalate esters (PAEs) plasticizers are environmental pollutants associated with reproductive toxicity, cancer risks, and birth defects. Vegetable oils are prone to PAEs contamination. In order to provide a reference for advancing PAEs detection methods, the pre-treatment methods and quantitative detection technologies of PAEs detection were reviewed, and their advantages and disadvantages were compared. The development trends of detection technology of PAEs were prospected. The pre-treatment methods of PAEs detection includes liquid-liquid extraction, solid-phase extraction, gel permeation chromatography, and QuEChERS, etc. The quantitative detection technologies for PAEs in vegetable oils include high-performance liquid chromatography, gas chromatography, liquid chromatography-mass spectrometry, gas chromatography-mass spectrometry, etc. Future directions in PAEs detection technology are expected to focus on the integration of combined pre-treatment approaches, online purification, microextraction techniques, and gas chromatography-tandem triple-quadrupole mass spectrometry (GC-MS/MS).
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