Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics

The growing demand for dermocosmetics with ingredients of natural origin reflects the pivotal role of cutaneous health and appearance in consumer self-esteem. Under this context, clays have attracted attention for their potential applications in dermatological care. Our research work aimed to increa...

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發表在:Cosmetics
Main Authors: Fernanda Daud Sarruf, Michele Georges Issa, Maria Valéria Robles Velasco, Catarina Rosado, André Rolim Baby
格式: Article
語言:英语
出版: MDPI AG 2025-10-01
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在線閱讀:https://www.mdpi.com/2079-9284/12/5/219
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author Fernanda Daud Sarruf
Michele Georges Issa
Maria Valéria Robles Velasco
Catarina Rosado
André Rolim Baby
author_facet Fernanda Daud Sarruf
Michele Georges Issa
Maria Valéria Robles Velasco
Catarina Rosado
André Rolim Baby
author_sort Fernanda Daud Sarruf
collection DOAJ
container_title Cosmetics
description The growing demand for dermocosmetics with ingredients of natural origin reflects the pivotal role of cutaneous health and appearance in consumer self-esteem. Under this context, clays have attracted attention for their potential applications in dermatological care. Our research work aimed to increase knowledge on the short-term impact of cosmetic formulations containing a blend of red, green, and black clays, assessing their effects on sebum regulation and in cutaneous biomechanical behavior (firmness/elasticity). Unlike daily skincare products, clay masks are used infrequently and for short durations; thus, an in vivo assessment was conducted after a 2-h application to reflect typical consumer use. The mineralogical and physicochemical properties of the different clays were characterized. Mineralogical analysis revealed distinct compositions among the clays: black clay exhibited a simpler mineral profile, lower density, and smaller particle size; green clay contained expandable smectite and was the densest; and red clay displayed the largest average particle size and highest iron content. Thermal analysis identified two major transitions: dehydration and kaolinite dehydroxylation. In vivo studies conducted in participants showed a significant reduction in skin oiliness across all clay-based formulations compared to baseline, control, and placebo following a 2-h application, and the rebound sebum production was dependent on clay concentration. Cutometry measurements did not reveal statistically significant improvements in skin firmness or elasticity compared to the control and placebo. The findings suggested that while clay-based formulations effectively reduced skin oiliness in the short term, their impact on sebum regulation and on skin biomechanical properties was limited after such a short product application period. Additional studies are warranted to elucidate the distinct effects of each clay, assess their behavior in different formulation bases, and evaluate their efficacy after repeated use.
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spelling doaj-art-e44f2c7eafe9407498ef3f9c7db1f3be2025-10-28T16:37:41ZengMDPI AGCosmetics2079-92842025-10-0112521910.3390/cosmetics12050219Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin BiomechanicsFernanda Daud Sarruf0Michele Georges Issa1Maria Valéria Robles Velasco2Catarina Rosado3André Rolim Baby4Department of Pharmacy, Faculty of Pharmaceutical Sciences, University of São Paulo, São Paulo 05508-000, BrazilDepartment of Pharmacy, Faculty of Pharmaceutical Sciences, University of São Paulo, São Paulo 05508-000, BrazilDepartment of Pharmacy, Faculty of Pharmaceutical Sciences, University of São Paulo, São Paulo 05508-000, BrazilCBIOS-Research Center for Biosciences and Health Technologies, Lusófona University, 1749-024 Lisbon, PortugalDepartment of Pharmacy, Faculty of Pharmaceutical Sciences, University of São Paulo, São Paulo 05508-000, BrazilThe growing demand for dermocosmetics with ingredients of natural origin reflects the pivotal role of cutaneous health and appearance in consumer self-esteem. Under this context, clays have attracted attention for their potential applications in dermatological care. Our research work aimed to increase knowledge on the short-term impact of cosmetic formulations containing a blend of red, green, and black clays, assessing their effects on sebum regulation and in cutaneous biomechanical behavior (firmness/elasticity). Unlike daily skincare products, clay masks are used infrequently and for short durations; thus, an in vivo assessment was conducted after a 2-h application to reflect typical consumer use. The mineralogical and physicochemical properties of the different clays were characterized. Mineralogical analysis revealed distinct compositions among the clays: black clay exhibited a simpler mineral profile, lower density, and smaller particle size; green clay contained expandable smectite and was the densest; and red clay displayed the largest average particle size and highest iron content. Thermal analysis identified two major transitions: dehydration and kaolinite dehydroxylation. In vivo studies conducted in participants showed a significant reduction in skin oiliness across all clay-based formulations compared to baseline, control, and placebo following a 2-h application, and the rebound sebum production was dependent on clay concentration. Cutometry measurements did not reveal statistically significant improvements in skin firmness or elasticity compared to the control and placebo. The findings suggested that while clay-based formulations effectively reduced skin oiliness in the short term, their impact on sebum regulation and on skin biomechanical properties was limited after such a short product application period. Additional studies are warranted to elucidate the distinct effects of each clay, assess their behavior in different formulation bases, and evaluate their efficacy after repeated use.https://www.mdpi.com/2079-9284/12/5/219clayssebumetrycutometrythermal analysismineralogical analysis
spellingShingle Fernanda Daud Sarruf
Michele Georges Issa
Maria Valéria Robles Velasco
Catarina Rosado
André Rolim Baby
Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics
clays
sebumetry
cutometry
thermal analysis
mineralogical analysis
title Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics
title_full Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics
title_fullStr Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics
title_full_unstemmed Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics
title_short Clay-Based Cosmetic Formulations: Mineralogical Properties and Short-Term Effects on Sebum Regulation and Skin Biomechanics
title_sort clay based cosmetic formulations mineralogical properties and short term effects on sebum regulation and skin biomechanics
topic clays
sebumetry
cutometry
thermal analysis
mineralogical analysis
url https://www.mdpi.com/2079-9284/12/5/219
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