Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate

Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate

The title compound, C14H28N2O5S, was synthesized by the reaction of 2-[(methylsulfanyl)methyl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen bonds into supramolecular chains propagating along the b-axis direction.

Bibliographic Details
Main Authors: Xiao-Guang Bai, Xiao-Yu Yang, Ju-Xian Wang
Format: Article
Language:English
Published: International Union of Crystallography 2014-08-01
Series:Acta Crystallographica Section E
Subjects:
crystal structure
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536814015062
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spelling doaj-0c006ef8c3ae4c68bc2b686d8c428c162020-11-24T21:25:55ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-08-01708o843o84310.1107/S1600536814015062xu5797Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylateXiao-Guang Bai0Xiao-Yu Yang1Ju-Xian Wang2Institute of Medicinal Biotechnology, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, People's Republic of ChinaHangDeXin (Beijing) Pharmatech. Co. Ltd, Fengtai District, Beijing 100050, People's Republic of ChinaInstitute of Medicinal Biotechnology, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, People's Republic of ChinaThe title compound, C14H28N2O5S, was synthesized by the reaction of 2-[(methylsulfanyl)methyl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen bonds into supramolecular chains propagating along the b-axis direction.http://scripts.iucr.org/cgi-bin/paper?S1600536814015062crystal structure
collection DOAJ
language English
format Article
sources DOAJ
author Xiao-Guang Bai
Xiao-Yu Yang
Ju-Xian Wang
spellingShingle Xiao-Guang Bai
Xiao-Yu Yang
Ju-Xian Wang
Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
Acta Crystallographica Section E
crystal structure
author_facet Xiao-Guang Bai
Xiao-Yu Yang
Ju-Xian Wang
author_sort Xiao-Guang Bai
title Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
title_short Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
title_full Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
title_fullStr Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
title_full_unstemmed Di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
title_sort di-tert-butyl 1-[2-hydroxy-3-(methylsulfanyl)propyl]hydrazine-1,2-dicarboxylate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2014-08-01
description The title compound, C14H28N2O5S, was synthesized by the reaction of 2-[(methylsulfanyl)methyl]oxirane with di-tert-butyl oxalate in hydrazine hydrate. In the crystal, molecules are linked by N—H...O and O—H...O hydrogen bonds into supramolecular chains propagating along the b-axis direction.
topic crystal structure
url http://scripts.iucr.org/cgi-bin/paper?S1600536814015062
work_keys_str_mv AT xiaoguangbai ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate
AT xiaoyuyang ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate
AT juxianwang ditertbutyl12hydroxy3methylsulfanylpropylhydrazine12dicarboxylate
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