Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil

<p>The CaOZnO nanoparticle catalysts with Ca to Zn atomic ratios of 0.08 and 0.25 have been successfully synthesized by co-precipitation method. The catalyst was characterized by X-ray Diffraction (XRD) analysis provided with Rietica and Maud software, Scanning Electron Microscopy (SEM) and Fo...

Full description

Bibliographic Details
Main Authors: Cicik Herlina Yulianti, Ratna Ediati, Djoko Hartanto, Tri Esti Purbaningtias, Yoshifumi Chisaki, Aishah Abdul Jalil, Che Ku Nor Liana Che Ku Hitam, Didik Prasetyoko
Format: Article
Language:English
Published: Diponegoro University 2014-07-01
Series:Bulletin of Chemical Reaction Engineering & Catalysis
Subjects:
Online Access:http://ejournal.undip.ac.id/index.php/bcrec/article/view/5998
id doaj-0fdd9307bf4a41e18576480bd2ff8b21
record_format Article
spelling doaj-0fdd9307bf4a41e18576480bd2ff8b212020-11-24T23:26:30ZengDiponegoro UniversityBulletin of Chemical Reaction Engineering & Catalysis1978-29932014-07-019210011010.9767/bcrec.9.2.5998.100-1105711Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm OilCicik Herlina Yulianti0Ratna Ediati1Djoko Hartanto2Tri Esti Purbaningtias3Yoshifumi Chisaki4Aishah Abdul Jalil5Che Ku Nor Liana Che Ku Hitam6Didik Prasetyoko7Department of Electrical Engineering, Faculty of Technology, Universitas Islam Lamongan, East Java,Laboratory of Material Chemistry and Energy, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Institut Teknologi Sepuluh Nopember, Surabaya,Laboratory of Material Chemistry and Energy, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Institut Teknologi Sepuluh Nopember, Surabaya,Diploma of Analytical Chemistry, Faculty of Mathematics and Natural Sciences, Islamic University of Indonesia, Yogyakarta,Department of Computer Science, Kumamoto University, 2-39-1 Kurokami, Kumamoto, 860-8555,Institute of Hydrogen Economy, Department of Chemical Engineering, Faculty of Chemical Engineering, Universiti Teknologi Malaysia, 81310 UTM, Johor Bahru,Institute of Hydrogen Economy, Department of Chemical Engineering, Faculty of Chemical Engineering, Universiti Teknologi Malaysia, 81310 UTM, Johor Bahru,Laboratory of Material Chemistry and Energy, Department of Chemistry, Faculty of Mathematics and Natural Sciences, Institut Teknologi Sepuluh Nopember, Surabaya,<p>The CaOZnO nanoparticle catalysts with Ca to Zn atomic ratios of 0.08 and 0.25 have been successfully synthesized by co-precipitation method. The catalyst was characterized by X-ray Diffraction (XRD) analysis provided with Rietica and Maud software, Scanning Electron Microscopy (SEM) and Fourier Transform Infrared spectroscopy (FT-IR), and its properties was compared with bare CaO and ZnO catalysts. The phase composition estimated by Rietica software revealed that the CaO catalyst consists of CaO and CaCO3 phases. The estimation of the particle size by Maud software, showed that the particle size of all catalysts increased by the following order: ZnO. © 2014 BCREC UNDIP. All rights reserved</p><p><em>Received: 1st January 2014; Revised: 10th March 2014; Accepted: 18th March 2014</em></p><p>[<strong>How to Cite</strong>: Yulianti, C.H., Ediati, R., Hartanto, D., Purbaningtias, T.E., Chisaki, Y., Jalil, A.A., Hitam, C.K.N.L.C.K., Prasetyoko, D., (2014). Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil. <em><strong>Bulletin of Chemical Reaction Engineering &amp; Catalysis</strong></em>, 9 (2): 100-110. (doi:10.9767/bcrec.9.2.5998.100-110)]</p><p><br />[<strong>Permalink/DOI</strong>: <a href="http://dx.doi.org/10.9767/bcrec.9.2.5998.100-110">http://dx.doi.org/10.9767/bcrec.9.2.5998.100-110</a>]</p>http://ejournal.undip.ac.id/index.php/bcrec/article/view/5998CaOZnO coprecipitationtransesterificationrefined palm oilyield of methyl esterTON-TOF
collection DOAJ
language English
format Article
sources DOAJ
author Cicik Herlina Yulianti
Ratna Ediati
Djoko Hartanto
Tri Esti Purbaningtias
Yoshifumi Chisaki
Aishah Abdul Jalil
Che Ku Nor Liana Che Ku Hitam
Didik Prasetyoko
spellingShingle Cicik Herlina Yulianti
Ratna Ediati
Djoko Hartanto
Tri Esti Purbaningtias
Yoshifumi Chisaki
Aishah Abdul Jalil
Che Ku Nor Liana Che Ku Hitam
Didik Prasetyoko
Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil
Bulletin of Chemical Reaction Engineering & Catalysis
CaOZnO coprecipitation
transesterification
refined palm oil
yield of methyl ester
TON-TOF
author_facet Cicik Herlina Yulianti
Ratna Ediati
Djoko Hartanto
Tri Esti Purbaningtias
Yoshifumi Chisaki
Aishah Abdul Jalil
Che Ku Nor Liana Che Ku Hitam
Didik Prasetyoko
author_sort Cicik Herlina Yulianti
title Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil
title_short Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil
title_full Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil
title_fullStr Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil
title_full_unstemmed Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil
title_sort synthesis of caozno nanoparticles catalyst and its application in transesterification of refined palm oil
publisher Diponegoro University
series Bulletin of Chemical Reaction Engineering & Catalysis
issn 1978-2993
publishDate 2014-07-01
description <p>The CaOZnO nanoparticle catalysts with Ca to Zn atomic ratios of 0.08 and 0.25 have been successfully synthesized by co-precipitation method. The catalyst was characterized by X-ray Diffraction (XRD) analysis provided with Rietica and Maud software, Scanning Electron Microscopy (SEM) and Fourier Transform Infrared spectroscopy (FT-IR), and its properties was compared with bare CaO and ZnO catalysts. The phase composition estimated by Rietica software revealed that the CaO catalyst consists of CaO and CaCO3 phases. The estimation of the particle size by Maud software, showed that the particle size of all catalysts increased by the following order: ZnO. © 2014 BCREC UNDIP. All rights reserved</p><p><em>Received: 1st January 2014; Revised: 10th March 2014; Accepted: 18th March 2014</em></p><p>[<strong>How to Cite</strong>: Yulianti, C.H., Ediati, R., Hartanto, D., Purbaningtias, T.E., Chisaki, Y., Jalil, A.A., Hitam, C.K.N.L.C.K., Prasetyoko, D., (2014). Synthesis of CaOZnO Nanoparticles Catalyst and Its Application in Transesterification of Refined Palm Oil. <em><strong>Bulletin of Chemical Reaction Engineering &amp; Catalysis</strong></em>, 9 (2): 100-110. (doi:10.9767/bcrec.9.2.5998.100-110)]</p><p><br />[<strong>Permalink/DOI</strong>: <a href="http://dx.doi.org/10.9767/bcrec.9.2.5998.100-110">http://dx.doi.org/10.9767/bcrec.9.2.5998.100-110</a>]</p>
topic CaOZnO coprecipitation
transesterification
refined palm oil
yield of methyl ester
TON-TOF
url http://ejournal.undip.ac.id/index.php/bcrec/article/view/5998
work_keys_str_mv AT cicikherlinayulianti synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT ratnaediati synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT djokohartanto synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT triestipurbaningtias synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT yoshifumichisaki synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT aishahabduljalil synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT chekunorlianachekuhitam synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
AT didikprasetyoko synthesisofcaoznonanoparticlescatalystanditsapplicationintransesterificationofrefinedpalmoil
_version_ 1725554851465658368