Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles

Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles

Fe3O4@SiO2-L-proline nanoparticles have been used as an effective catalyst for the preparation of pyrimidines by three-component reactions of 1,3-dimethylbarbituric acid, aromatic aldehydes and 4-methyl aniline or 4-methoxy aniline under reflux condition in ethanol. Fe3O4@SiO2-L-proline nanoparticle...

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Main Authors: Safaei-Ghomi Javad, Samadi Zahra
Format: Article
Language:English
Published: De Gruyter 2020-07-01
Series:Main Group Metal Chemistry
Subjects:
pyrimidines
fe3o4 nanoparticles
heterogeneous catalyst
one-pot
Online Access:https://doi.org/10.1515/mgmc-2020-0014
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spelling doaj-13edfff23bbf4e5e98f2e50e4e1fa92e2021-10-02T19:24:45ZengDe GruyterMain Group Metal Chemistry0792-12412191-02192020-07-0143111712410.1515/mgmc-2020-0014mgmc-2020-0014Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticlesSafaei-Ghomi Javad0Samadi Zahra1Department of Organic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P.O. Box 87317-51167, I. R. IranDepartment of Organic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P.O. Box 87317-51167, I. R. IranFe3O4@SiO2-L-proline nanoparticles have been used as an effective catalyst for the preparation of pyrimidines by three-component reactions of 1,3-dimethylbarbituric acid, aromatic aldehydes and 4-methyl aniline or 4-methoxy aniline under reflux condition in ethanol. Fe3O4@SiO2-L-proline nanoparticles have been characterized by scanning electronic microscopy (SEM), powder X-ray diffraction (XRD), vibrating sample magnetometer (VSM), thermal gravimetric analysis (TGA), energy dispersive X-ray (EDS), dynamic light scattering (DLS) and FT-IR spectroscopy. This method provides several advantages including, the reusability of the catalyst, low catalyst loading, atom economy, short reaction times and high yields of products.https://doi.org/10.1515/mgmc-2020-0014pyrimidinesfe3o4 nanoparticlesheterogeneous catalystone-pot
collection DOAJ
language English
format Article
sources DOAJ
author Safaei-Ghomi Javad
Samadi Zahra
spellingShingle Safaei-Ghomi Javad
Samadi Zahra
Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles
Main Group Metal Chemistry
pyrimidines
fe3o4 nanoparticles
heterogeneous catalyst
one-pot
author_facet Safaei-Ghomi Javad
Samadi Zahra
author_sort Safaei-Ghomi Javad
title Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles
title_short Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles
title_full Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles
title_fullStr Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles
title_full_unstemmed Synthesis of pyrimidines by Fe3O4@SiO2-L-proline nanoparticles
title_sort synthesis of pyrimidines by fe3o4@sio2-l-proline nanoparticles
publisher De Gruyter
series Main Group Metal Chemistry
issn 0792-1241
2191-0219
publishDate 2020-07-01
description Fe3O4@SiO2-L-proline nanoparticles have been used as an effective catalyst for the preparation of pyrimidines by three-component reactions of 1,3-dimethylbarbituric acid, aromatic aldehydes and 4-methyl aniline or 4-methoxy aniline under reflux condition in ethanol. Fe3O4@SiO2-L-proline nanoparticles have been characterized by scanning electronic microscopy (SEM), powder X-ray diffraction (XRD), vibrating sample magnetometer (VSM), thermal gravimetric analysis (TGA), energy dispersive X-ray (EDS), dynamic light scattering (DLS) and FT-IR spectroscopy. This method provides several advantages including, the reusability of the catalyst, low catalyst loading, atom economy, short reaction times and high yields of products.
topic pyrimidines
fe3o4 nanoparticles
heterogeneous catalyst
one-pot
url https://doi.org/10.1515/mgmc-2020-0014
work_keys_str_mv AT safaeighomijavad synthesisofpyrimidinesbyfe3o4sio2lprolinenanoparticles
AT samadizahra synthesisofpyrimidinesbyfe3o4sio2lprolinenanoparticles
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