1-Fluoro-2,5-dimethoxy-4-nitrobenzene
1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR.
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Online Access: | http://www.mdpi.com/1422-8599/2018/1/M984 |
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doaj-1578ce90181644a1bf0fe791c47eb0dc2020-11-24T21:39:36ZengMDPI AGMolbank1422-85992018-02-0120181M98410.3390/M984M9841-Fluoro-2,5-dimethoxy-4-nitrobenzeneMartin Sweeney0Patrick McArdle1Fawaz Aldabbagh2School of Chemistry, National University of Ireland Galway, University Road, Galway, H91 TK33, IrelandSchool of Chemistry, National University of Ireland Galway, University Road, Galway, H91 TK33, IrelandSchool of Chemistry, National University of Ireland Galway, University Road, Galway, H91 TK33, Ireland1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR.http://www.mdpi.com/1422-8599/2018/1/M984X-ray crystallographyfluorobenzenenitrationnucleophilic aromatic substitution |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Martin Sweeney Patrick McArdle Fawaz Aldabbagh |
spellingShingle |
Martin Sweeney Patrick McArdle Fawaz Aldabbagh 1-Fluoro-2,5-dimethoxy-4-nitrobenzene Molbank X-ray crystallography fluorobenzene nitration nucleophilic aromatic substitution |
author_facet |
Martin Sweeney Patrick McArdle Fawaz Aldabbagh |
author_sort |
Martin Sweeney |
title |
1-Fluoro-2,5-dimethoxy-4-nitrobenzene |
title_short |
1-Fluoro-2,5-dimethoxy-4-nitrobenzene |
title_full |
1-Fluoro-2,5-dimethoxy-4-nitrobenzene |
title_fullStr |
1-Fluoro-2,5-dimethoxy-4-nitrobenzene |
title_full_unstemmed |
1-Fluoro-2,5-dimethoxy-4-nitrobenzene |
title_sort |
1-fluoro-2,5-dimethoxy-4-nitrobenzene |
publisher |
MDPI AG |
series |
Molbank |
issn |
1422-8599 |
publishDate |
2018-02-01 |
description |
1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR. |
topic |
X-ray crystallography fluorobenzene nitration nucleophilic aromatic substitution |
url |
http://www.mdpi.com/1422-8599/2018/1/M984 |
work_keys_str_mv |
AT martinsweeney 1fluoro25dimethoxy4nitrobenzene AT patrickmcardle 1fluoro25dimethoxy4nitrobenzene AT fawazaldabbagh 1fluoro25dimethoxy4nitrobenzene |
_version_ |
1725930280069365760 |