1-Fluoro-2,5-dimethoxy-4-nitrobenzene

1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR.

Bibliographic Details
Main Authors: Martin Sweeney, Patrick McArdle, Fawaz Aldabbagh
Format: Article
Language:English
Published: MDPI AG 2018-02-01
Series:Molbank
Subjects:
Online Access:http://www.mdpi.com/1422-8599/2018/1/M984
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spelling doaj-1578ce90181644a1bf0fe791c47eb0dc2020-11-24T21:39:36ZengMDPI AGMolbank1422-85992018-02-0120181M98410.3390/M984M9841-Fluoro-2,5-dimethoxy-4-nitrobenzeneMartin Sweeney0Patrick McArdle1Fawaz Aldabbagh2School of Chemistry, National University of Ireland Galway, University Road, Galway, H91 TK33, IrelandSchool of Chemistry, National University of Ireland Galway, University Road, Galway, H91 TK33, IrelandSchool of Chemistry, National University of Ireland Galway, University Road, Galway, H91 TK33, Ireland1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR.http://www.mdpi.com/1422-8599/2018/1/M984X-ray crystallographyfluorobenzenenitrationnucleophilic aromatic substitution
collection DOAJ
language English
format Article
sources DOAJ
author Martin Sweeney
Patrick McArdle
Fawaz Aldabbagh
spellingShingle Martin Sweeney
Patrick McArdle
Fawaz Aldabbagh
1-Fluoro-2,5-dimethoxy-4-nitrobenzene
Molbank
X-ray crystallography
fluorobenzene
nitration
nucleophilic aromatic substitution
author_facet Martin Sweeney
Patrick McArdle
Fawaz Aldabbagh
author_sort Martin Sweeney
title 1-Fluoro-2,5-dimethoxy-4-nitrobenzene
title_short 1-Fluoro-2,5-dimethoxy-4-nitrobenzene
title_full 1-Fluoro-2,5-dimethoxy-4-nitrobenzene
title_fullStr 1-Fluoro-2,5-dimethoxy-4-nitrobenzene
title_full_unstemmed 1-Fluoro-2,5-dimethoxy-4-nitrobenzene
title_sort 1-fluoro-2,5-dimethoxy-4-nitrobenzene
publisher MDPI AG
series Molbank
issn 1422-8599
publishDate 2018-02-01
description 1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR.
topic X-ray crystallography
fluorobenzene
nitration
nucleophilic aromatic substitution
url http://www.mdpi.com/1422-8599/2018/1/M984
work_keys_str_mv AT martinsweeney 1fluoro25dimethoxy4nitrobenzene
AT patrickmcardle 1fluoro25dimethoxy4nitrobenzene
AT fawazaldabbagh 1fluoro25dimethoxy4nitrobenzene
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