PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR
In this work, prediction models of Saturates, Aromatics, Resins and Asphaltenes fractions (SARA) from thirty-seven vacuum residues of representative Colombian crudes and eighteen fractions of molecular distillation process were obtained. Mid-Infrared (MIR) Attenuated Total Reflection (ATR) spectro...
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Universidad Industrial de Santander
2014-06-01
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doaj-16f3d7f62f0d46008bdf03ec2bb182692020-11-24T21:36:55ZengUniversidad Industrial de SantanderRevista Ion0120-100X2145-84802014-06-012714348PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATRJorge A. Orrego-Ruiz0Rafael Cabanzo1Enrique Mejía-Ospino2ECOPETROL S.AUniversidad Industrial de SantanderUniversidad Industrial de SantanderIn this work, prediction models of Saturates, Aromatics, Resins and Asphaltenes fractions (SARA) from thirty-seven vacuum residues of representative Colombian crudes and eighteen fractions of molecular distillation process were obtained. Mid-Infrared (MIR) Attenuated Total Reflection (ATR) spectroscopy in combination with partial least squares (PLS) regression analysis was used to estimate accurately SARA analysis in these kind of samples. Calibration coefficients of prediction models were for saturates, aromatics, resins and asphaltenes fractions, 0.99, 0.96, 0.97 and 0.99, respectively. This methodology permits to control the molecular distillation process since small differences in chemical composition can be detected. Total time elapsed to give the SARA analysis per sample is 10 minutes.http://revistas.uis.edu.co/index.php/revistaion/article/view/4144/4462MIR-ATRPLSSARA analysismolecular distillationvacuum residue |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Jorge A. Orrego-Ruiz Rafael Cabanzo Enrique Mejía-Ospino |
spellingShingle |
Jorge A. Orrego-Ruiz Rafael Cabanzo Enrique Mejía-Ospino PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR Revista Ion MIR-ATR PLS SARA analysis molecular distillation vacuum residue |
author_facet |
Jorge A. Orrego-Ruiz Rafael Cabanzo Enrique Mejía-Ospino |
author_sort |
Jorge A. Orrego-Ruiz |
title |
PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR |
title_short |
PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR |
title_full |
PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR |
title_fullStr |
PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR |
title_full_unstemmed |
PLS models for determination of SARA analysis of Colombian vacuum residues and molecular distillation fractions using MIR-ATR |
title_sort |
pls models for determination of sara analysis of colombian vacuum residues and molecular distillation fractions using mir-atr |
publisher |
Universidad Industrial de Santander |
series |
Revista Ion |
issn |
0120-100X 2145-8480 |
publishDate |
2014-06-01 |
description |
In this work, prediction models of Saturates, Aromatics, Resins and Asphaltenes fractions (SARA) from
thirty-seven vacuum residues of representative Colombian crudes and eighteen fractions of molecular
distillation process were obtained. Mid-Infrared (MIR) Attenuated Total Reflection (ATR) spectroscopy
in combination with partial least squares (PLS) regression analysis was used to estimate accurately
SARA analysis in these kind of samples. Calibration coefficients of prediction models were for saturates,
aromatics, resins and asphaltenes fractions, 0.99, 0.96, 0.97 and 0.99, respectively. This methodology
permits to control the molecular distillation process since small differences in chemical composition can
be detected. Total time elapsed to give the SARA analysis per sample is 10 minutes. |
topic |
MIR-ATR PLS SARA analysis molecular distillation vacuum residue |
url |
http://revistas.uis.edu.co/index.php/revistaion/article/view/4144/4462 |
work_keys_str_mv |
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