Biolubricant Production through Double Transesterification: Reactor Design for the Implementation of a Biorefinery Based on Rapeseed

• Main Authors: José María Encinar, Sergio Nogales-Delgado, Antonio Pinilla
• Format: Article
• Language: English
• Published: MDPI AG 2021-07-01
• Series: Processes
• Subjects: Brassica Napus; fatty acid methyl esters; 2-Ethyl-2-hydroxymethyl-1,3-propanediol; viscosity; batch reactor; kinetics
• Online Access: https://www.mdpi.com/2227-9717/9/7/1224

The production and use of biolubricants as replacements for mineral lubricants align with the promotion of sustainable development goals, contributing to the sustainable economic growth of developing countries as well as the preservation of the environment. The implementation of biorefineries (where the production of biolubricants through transesterification could play an important role) is becoming important for these purposes, using natural feedstocks such as rapeseed, which is an interesting crop that can adapt to different climates under extreme weather conditions. The aim of this research work was to study the design of a reactor to produce rapeseed biolubricant through double transesterification of the corresponding vegetable oil. Thus, the kinetics to design a reactor was studied, sizing it according to the properties of the biolubricant and the demand in Spain. As a result, a SAE 10W30 biolubricant was obtained, which was suitable for Diesel engines. A batch reactor was selected for the production of this biolubricant at a national level, with a pseudo-first reaction order and a reactor volume of 9.66 m³.