| Summary: | In this study, high-purity V2CTx MXene was successfully synthesized by etching V2AlC with fluoride and hydrochloric acid mixed solution using a hydrothermal-assisted method. This method is more concise and effective and has a low level of danger. The morphology and structure of the V2CTx MXene was characterized by X-ray diffraction, field emission scanning electron microscopy, and X-ray photoelectron spectroscopy. The electrochemical properties were investigated as an anode material for lithium ion batteries. The results show that the prepared V2CTx had a higher purity and showed excellent electrochemical properties as an anode of lithium-ion batteries. And V2CTx prepared with different etching system can he obtained with high yield and excellent purity by changing the reactive conditions of the system. However, electrochemical performance of V2CTx MXene obtained at different etching system is quite different. V2CTx synthesized in the mixed solution of ammonium fluoride and hydrochloric acid has the best performance, which originates from more accessible active sites for ion in the enlarged interlayer distance, and the smaller impedance of V2CTx. Keywords: MXene, V2CTx, Hydrothermal, Lithium ion battery
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