Tris(naphthalen-1-yl)phosphane chloroform hemisolvate

Tris(naphthalen-1-yl)phosphane chloroform hemisolvate

The title compound, P(C10H7)3·0.5CHCl3, was isolated after the unsuccessful reaction of KSeCN and tris(naphthalen-1-yl)phosphane. The solvent molecule is disordered about an inversion center. The effective cone angle of the phosphine is 203°. In the crystal, weak C&...

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Bibliographic Details
Main Authors: Wade L. Davis, Alfred Muller
Format: Article
Language:English
Published: International Union of Crystallography 2012-12-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812048234
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spelling doaj-2e521d8d908c4552b3ef60e139d5b47b2020-11-25T00:50:37ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-12-016812o3484o348410.1107/S1600536812048234Tris(naphthalen-1-yl)phosphane chloroform hemisolvateWade L. DavisAlfred MullerThe title compound, P(C10H7)3·0.5CHCl3, was isolated after the unsuccessful reaction of KSeCN and tris(naphthalen-1-yl)phosphane. The solvent molecule is disordered about an inversion center. The effective cone angle of the phosphine is 203°. In the crystal, weak C—H...Cl and C—H...π interactions are observed.http://scripts.iucr.org/cgi-bin/paper?S1600536812048234
collection DOAJ
language English
format Article
sources DOAJ
author Wade L. Davis
Alfred Muller
spellingShingle Wade L. Davis
Alfred Muller
Tris(naphthalen-1-yl)phosphane chloroform hemisolvate
Acta Crystallographica Section E
author_facet Wade L. Davis
Alfred Muller
author_sort Wade L. Davis
title Tris(naphthalen-1-yl)phosphane chloroform hemisolvate
title_short Tris(naphthalen-1-yl)phosphane chloroform hemisolvate
title_full Tris(naphthalen-1-yl)phosphane chloroform hemisolvate
title_fullStr Tris(naphthalen-1-yl)phosphane chloroform hemisolvate
title_full_unstemmed Tris(naphthalen-1-yl)phosphane chloroform hemisolvate
title_sort tris(naphthalen-1-yl)phosphane chloroform hemisolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-12-01
description The title compound, P(C10H7)3·0.5CHCl3, was isolated after the unsuccessful reaction of KSeCN and tris(naphthalen-1-yl)phosphane. The solvent molecule is disordered about an inversion center. The effective cone angle of the phosphine is 203°. In the crystal, weak C—H...Cl and C—H...π interactions are observed.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812048234
work_keys_str_mv AT wadeldavis trisnaphthalen1ylphosphanechloroformhemisolvate
AT alfredmuller trisnaphthalen1ylphosphanechloroformhemisolvate
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