Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques

Karanjin is the medicinal drug that used as anti- inflammatory and anti-cancer. The object of this study is to isolate karanjin in karanja (pongamia pinnata Linn.) seed oil. The seed oil was subjected to triple petroleum with continuously constant shaking for first 48 hours, 24 hours for each second...

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Main Authors: Sushil Kumar Dhanmane, Faisal A. Salih
Format: Article
Language:English
Published: Sulaimani Polytechnic University 2018-07-01
Series:Kurdistan Journal of Applied Research
Subjects:
Online Access:http://kjar.spu.edu.iq/index.php/kjar/article/view/216
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spelling doaj-34434ab238004c7aae2eba77c3cc60b32020-11-25T00:37:12ZengSulaimani Polytechnic UniversityKurdistan Journal of Applied Research2411-76842411-77062018-07-0115616010.24017/science.2018.2.26216Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical TechniquesSushil Kumar Dhanmane0Faisal A. Salih1Chemistry, Fergusson College, Savitribai Phule, Pune University, Pune , IndiaMedical Laboratory, Technical College of Health, Sulaimani Polytechnic University, Sulaymaniyah , Kurdistan region , IraqKaranjin is the medicinal drug that used as anti- inflammatory and anti-cancer. The object of this study is to isolate karanjin in karanja (pongamia pinnata Linn.) seed oil. The seed oil was subjected to triple petroleum with continuously constant shaking for first 48 hours, 24 hours for each second and third extraction then separated under reduced pressure at 50˚C on rotatory evaporate to get yellow viscous oil. Separate non-fatty components using ethanol solvent and reduced under 50˚C with pressure to get (43.33 g) yellow oil. The oil was kept for 3 days at 45˚C in refrigerator white deposited at bottom of oil, the residue recrystallized with methanol it should be done fast and carefully to prevent solubility of karanjin in methanol partially, the purity of isolated karanjin was found to be (99.623%). From TLC, HPL, IR, 1HNMR, 13CNMR spectra data, structure elucidation was done and the structure was confirmed as karanjin.http://kjar.spu.edu.iq/index.php/kjar/article/view/216Karanjin, pongamia pinnata, Karanja oil, medicinal plant.
collection DOAJ
language English
format Article
sources DOAJ
author Sushil Kumar Dhanmane
Faisal A. Salih
spellingShingle Sushil Kumar Dhanmane
Faisal A. Salih
Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques
Kurdistan Journal of Applied Research
Karanjin, pongamia pinnata, Karanja oil, medicinal plant.
author_facet Sushil Kumar Dhanmane
Faisal A. Salih
author_sort Sushil Kumar Dhanmane
title Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques
title_short Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques
title_full Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques
title_fullStr Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques
title_full_unstemmed Isolation of Karanjin from Pongamia Pinnata and Its Identification by Difference Analytical Techniques
title_sort isolation of karanjin from pongamia pinnata and its identification by difference analytical techniques
publisher Sulaimani Polytechnic University
series Kurdistan Journal of Applied Research
issn 2411-7684
2411-7706
publishDate 2018-07-01
description Karanjin is the medicinal drug that used as anti- inflammatory and anti-cancer. The object of this study is to isolate karanjin in karanja (pongamia pinnata Linn.) seed oil. The seed oil was subjected to triple petroleum with continuously constant shaking for first 48 hours, 24 hours for each second and third extraction then separated under reduced pressure at 50˚C on rotatory evaporate to get yellow viscous oil. Separate non-fatty components using ethanol solvent and reduced under 50˚C with pressure to get (43.33 g) yellow oil. The oil was kept for 3 days at 45˚C in refrigerator white deposited at bottom of oil, the residue recrystallized with methanol it should be done fast and carefully to prevent solubility of karanjin in methanol partially, the purity of isolated karanjin was found to be (99.623%). From TLC, HPL, IR, 1HNMR, 13CNMR spectra data, structure elucidation was done and the structure was confirmed as karanjin.
topic Karanjin, pongamia pinnata, Karanja oil, medicinal plant.
url http://kjar.spu.edu.iq/index.php/kjar/article/view/216
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AT faisalasalih isolationofkaranjinfrompongamiapinnataanditsidentificationbydifferenceanalyticaltechniques
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