(E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide

(E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide

The title Schiff base compound, C13H8Cl3N3O2, was synthesized by the condensation reaction of 3,5-dichlorosalicylaldehyde with 6-chloronicotinic acid hydrazide in 95% ethanol. The molecule is nearly planar, with a dihedral angle of 1.9 (2)° between the aromatic ring planes...

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Main Author: Chun-yan Ren
Format: Article
Language:English
Published: International Union of Crystallography 2009-04-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809007272
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spelling doaj-3aee27b1927c4502a7f7fd1c5021748c2020-11-24T21:32:33ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-04-01654o678o67810.1107/S1600536809007272(E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazideChun-yan RenThe title Schiff base compound, C13H8Cl3N3O2, was synthesized by the condensation reaction of 3,5-dichlorosalicylaldehyde with 6-chloronicotinic acid hydrazide in 95% ethanol. The molecule is nearly planar, with a dihedral angle of 1.9 (2)° between the aromatic ring planes, and an intramolecular O—H...N hydrogen bond is observed. In the crystal, the molecules are connected by intermolecular N—H...O hydrogen bonds into infinite chains propagating in [100]. http://scripts.iucr.org/cgi-bin/paper?S1600536809007272
collection DOAJ
language English
format Article
sources DOAJ
author Chun-yan Ren
spellingShingle Chun-yan Ren
(E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
Acta Crystallographica Section E
author_facet Chun-yan Ren
author_sort Chun-yan Ren
title (E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
title_short (E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
title_full (E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
title_fullStr (E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
title_full_unstemmed (E)-6-Chloro-N′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
title_sort (e)-6-chloro-n′-(3,5-dichloro-2-hydroxybenzylidene)nicotinohydrazide
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-04-01
description The title Schiff base compound, C13H8Cl3N3O2, was synthesized by the condensation reaction of 3,5-dichlorosalicylaldehyde with 6-chloronicotinic acid hydrazide in 95% ethanol. The molecule is nearly planar, with a dihedral angle of 1.9 (2)° between the aromatic ring planes, and an intramolecular O—H...N hydrogen bond is observed. In the crystal, the molecules are connected by intermolecular N—H...O hydrogen bonds into infinite chains propagating in [100].
url http://scripts.iucr.org/cgi-bin/paper?S1600536809007272
work_keys_str_mv AT chunyanren e6chloronamp824235dichloro2hydroxybenzylidenenicotinohydrazide
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