Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn

Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn

C18H28N2O4P2S4Zn, triclinic, P1̄ (no. 2), a = 15.2379(1) Å, b = 17.3322(2) Å, c = 21.8829(1) Å, α = 75.919(1)°, β = 78.050(1)°, γ = 68.170(1)°, V = 5159.97(8) Å3, Z = 8, Rgt(F) = 0.0246, wRref(F2) = 0.0681, T = 100 K.

Bibliographic Details
Main Authors: Tan Yee Seng, Tiekink Edward R.T.
Format: Article
Language:English
Published: De Gruyter 2019-12-01
Series:Zeitschrift für Kristallographie - New Crystal Structures
Subjects:
1957379
Online Access:https://doi.org/10.1515/ncrs-2019-0594
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spelling doaj-3cba23a2e23f44299005d0bf6d1d89a32021-09-06T19:20:58ZengDe GruyterZeitschrift für Kristallographie - New Crystal Structures1433-72662197-45782019-12-01235123323710.1515/ncrs-2019-0594Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4ZnTan Yee Seng0Tiekink Edward R.T.1Research Centre for Crystalline Materials, School of Science and Technology, Sunway University, 47500 Bandar Sunway, Selangor Darul Ehsan, MalaysiaResearch Centre for Crystalline Materials, School of Science and Technology, Sunway University, 47500 Bandar Sunway, Selangor Darul Ehsan, MalaysiaC18H28N2O4P2S4Zn, triclinic, P1̄ (no. 2), a = 15.2379(1) Å, b = 17.3322(2) Å, c = 21.8829(1) Å, α = 75.919(1)°, β = 78.050(1)°, γ = 68.170(1)°, V = 5159.97(8) Å3, Z = 8, Rgt(F) = 0.0246, wRref(F2) = 0.0681, T = 100 K.https://doi.org/10.1515/ncrs-2019-05941957379
collection DOAJ
language English
format Article
sources DOAJ
author Tan Yee Seng
Tiekink Edward R.T.
spellingShingle Tan Yee Seng
Tiekink Edward R.T.
Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn
Zeitschrift für Kristallographie - New Crystal Structures
1957379
author_facet Tan Yee Seng
Tiekink Edward R.T.
author_sort Tan Yee Seng
title Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn
title_short Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn
title_full Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn
title_fullStr Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn
title_full_unstemmed Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2N,N′)-bis(O,O′-diethyldithiophosphato-κ1S)zinc(II)], C18H28N2O4P2S4Zn
title_sort crystal structure of a low-temperature (100 k) polymorph of catena-poly[(μ2-4,4′-bipyridine-κ2n,n′)-bis(o,o′-diethyldithiophosphato-κ1s)zinc(ii)], c18h28n2o4p2s4zn
publisher De Gruyter
series Zeitschrift für Kristallographie - New Crystal Structures
issn 1433-7266
2197-4578
publishDate 2019-12-01
description C18H28N2O4P2S4Zn, triclinic, P1̄ (no. 2), a = 15.2379(1) Å, b = 17.3322(2) Å, c = 21.8829(1) Å, α = 75.919(1)°, β = 78.050(1)°, γ = 68.170(1)°, V = 5159.97(8) Å3, Z = 8, Rgt(F) = 0.0246, wRref(F2) = 0.0681, T = 100 K.
topic 1957379
url https://doi.org/10.1515/ncrs-2019-0594
work_keys_str_mv AT tanyeeseng crystalstructureofalowtemperature100kpolymorphofcatenapolym244bipyridinek2nnbisoodiethyldithiophosphatok1szinciic18h28n2o4p2s4zn
AT tiekinkedwardrt crystalstructureofalowtemperature100kpolymorphofcatenapolym244bipyridinek2nnbisoodiethyldithiophosphatok1szinciic18h28n2o4p2s4zn
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