Synthesis of Cu3N from CuO and NaNH2
We report on the low-temperature synthesis of submicron-sized Cu3N powder produced from CuO and NaNH2 powder mixture by heating at 150–190 °C in a Teflon-sealed autoclave. The structure was the anti-RuO3 type with a lattice parameter of 0.3814(1) nm, and strong optical absorption was observed below...
| Main Authors: | , , |
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| Format: | Article |
| Language: | English |
| Published: |
Taylor & Francis Group
2014-12-01
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| Series: | Journal of Asian Ceramic Societies |
| Subjects: | |
| Online Access: | http://www.sciencedirect.com/science/article/pii/S2187076414000876 |
| Summary: | We report on the low-temperature synthesis of submicron-sized Cu3N powder produced from CuO and NaNH2 powder mixture by heating at 150–190 °C in a Teflon-sealed autoclave. The structure was the anti-RuO3 type with a lattice parameter of 0.3814(1) nm, and strong optical absorption was observed below ∼1.9 eV. This synthesis method has the potential of facile control of the reaction with less use of ammonia sources. |
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| ISSN: | 2187-0764 |