Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol

In the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-dichloroaniline with 2,3-dihydroxybenzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°. Intramolecular O—H...O and O—H...N hydrogen bonds close S(5) and S(6) rings, respectively. In the crystal, inv...

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Main Authors:	Muhammad Nawaz Tahir, Hazoor Ahmad Shad, Abdul Rauf, Abdul Haleem Khan
Format:	Article
Language:	English
Published:	International Union of Crystallography 2015-02-01
Series:	Acta Crystallographica Section E: Crystallographic Communications
Subjects:	crystal structure benzene-1,2-diol Schiff base hydrogen bonding
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2056989015001401

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spelling	doaj-40f2ab6ab503448999b6848061284a932020-11-24T21:43:13ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902015-02-01712o137o13810.1107/S2056989015001401hb7353Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diolMuhammad Nawaz Tahir0Hazoor Ahmad Shad1Abdul Rauf2Abdul Haleem Khan3Department of Physics, University of Sargodha, Sargodha, Punjab, PakistanDepartment of Chemistry, University of Sargodha, Sargodha, PakistanDepartment of Chemistry, Chenab College, Jhang, Punjab, PakistanDrug Controller, Sir Ganga Ram Hospital, Lahore, PakistanIn the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-dichloroaniline with 2,3-dihydroxybenzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°. Intramolecular O—H...O and O—H...N hydrogen bonds close S(5) and S(6) rings, respectively. In the crystal, inversion dimers linked by pairs of O—H...O hydrogen bonds generate R22(10) loops. A weak C—H...π interaction is also observed.http://scripts.iucr.org/cgi-bin/paper?S2056989015001401crystal structurebenzene-1,2-diolSchiff basehydrogen bonding
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Muhammad Nawaz Tahir Hazoor Ahmad Shad Abdul Rauf Abdul Haleem Khan
spellingShingle	Muhammad Nawaz Tahir Hazoor Ahmad Shad Abdul Rauf Abdul Haleem Khan Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol Acta Crystallographica Section E: Crystallographic Communications crystal structure benzene-1,2-diol Schiff base hydrogen bonding
author_facet	Muhammad Nawaz Tahir Hazoor Ahmad Shad Abdul Rauf Abdul Haleem Khan
author_sort	Muhammad Nawaz Tahir
title	Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol
title_short	Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol
title_full	Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol
title_fullStr	Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol
title_full_unstemmed	Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol
title_sort	crystal structure of 3-{(e)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol
publisher	International Union of Crystallography
series	Acta Crystallographica Section E: Crystallographic Communications
issn	2056-9890
publishDate	2015-02-01
description	In the title Schiff base, C13H9Cl2NO2, which arose from the condensation of 3,4-dichloroaniline with 2,3-dihydroxybenzaldehyde, the dihedral angle between the aromatic rings is 44.74 (13)°. Intramolecular O—H...O and O—H...N hydrogen bonds close S(5) and S(6) rings, respectively. In the crystal, inversion dimers linked by pairs of O—H...O hydrogen bonds generate R22(10) loops. A weak C—H...π interaction is also observed.
topic	crystal structure benzene-1,2-diol Schiff base hydrogen bonding
url	http://scripts.iucr.org/cgi-bin/paper?S2056989015001401
work_keys_str_mv	AT muhammadnawaztahir crystalstructureof3e34dichlorophenyliminomethylbenzene12diol AT hazoorahmadshad crystalstructureof3e34dichlorophenyliminomethylbenzene12diol AT abdulrauf crystalstructureof3e34dichlorophenyliminomethylbenzene12diol AT abdulhaleemkhan crystalstructureof3e34dichlorophenyliminomethylbenzene12diol
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Crystal structure of 3-{(E)-[(3,4-dichlorophenyl)imino]methyl}benzene-1,2-diol

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