Polydisperse methyl β-cyclodextrin–epichlorohydrin polymers: variable contact time 13C CP-MAS solid-state NMR characterization

Polydisperse methyl β-cyclodextrin–epichlorohydrin polymers: variable contact time 13C CP-MAS solid-state NMR characterization

The polymerization of partially methylated β-cyclodextrin (CRYSMEB) with epichlorohydrin was carried out in the presence of a known amount of toluene as imprinting agent. Three different preparations (D1, D2 and D3) of imprinted polymers were obtained and characterized by solid-state 13C NMR spectro...

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Bibliographic Details
Main Authors: Isabelle Mallard, Davy Baudelet, Franca Castiglione, Monica Ferro, Walter Panzeri, Enzio Ragg, Andrea Mele
Format: Article
Language:English
Published: Beilstein-Institut 2015-12-01
Series:Beilstein Journal of Organic Chemistry
Subjects:
dynamic cross-polarization
epichlorohydrin
imprinted
insoluble CRYSMEB polymers
solid-state NMR spectroscopy
Online Access:https://doi.org/10.3762/bjoc.11.299

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