4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate

4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate

In the cation of the title salt, C9H13N2O2+·C7H3N2O6−, the piperazine ring adopts a slightly distorted chair conformation. Twofold rotational disorder is exhibited by the furan ring in a 0.430 (4):0.570 (4) ratio. In the crystal, N—H...O hydrogen bonds link the ions into chains along [010]. Addition...

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Main Authors: Channappa N. Kavitha, Manpreet Kaur, Jerry P. Jasinski, Ray J. Butcher, H.S. Yathirajan
Format: Article
Language:English
Published: International Union of Crystallography 2014-06-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S160053681401126X
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spelling doaj-44da5ad3daf64306910cb4a334e775b92020-11-24T21:25:00ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-06-01706o700o70110.1107/S160053681401126Xtk53144-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoateChannappa N. Kavitha0Manpreet Kaur1Jerry P. Jasinski2Ray J. Butcher3H.S. Yathirajan4Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, IndiaDepartment of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, IndiaDepartment of Chemistry, Keene State College, 229 Main Street, Keene, NH 03435-2001, USADepartment of Chemistry, Howard University, 525 College Street NW, Washington, DC 20059, USADepartment of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, IndiaIn the cation of the title salt, C9H13N2O2+·C7H3N2O6−, the piperazine ring adopts a slightly distorted chair conformation. Twofold rotational disorder is exhibited by the furan ring in a 0.430 (4):0.570 (4) ratio. In the crystal, N—H...O hydrogen bonds link the ions into chains along [010]. Additional weak C—H...O interactions are observed, leading to a supramolecular layer parallel to (011).http://scripts.iucr.org/cgi-bin/paper?S160053681401126X
collection DOAJ
language English
format Article
sources DOAJ
author Channappa N. Kavitha
Manpreet Kaur
Jerry P. Jasinski
Ray J. Butcher
H.S. Yathirajan
spellingShingle Channappa N. Kavitha
Manpreet Kaur
Jerry P. Jasinski
Ray J. Butcher
H.S. Yathirajan
4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
Acta Crystallographica Section E
author_facet Channappa N. Kavitha
Manpreet Kaur
Jerry P. Jasinski
Ray J. Butcher
H.S. Yathirajan
author_sort Channappa N. Kavitha
title 4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
title_short 4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
title_full 4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
title_fullStr 4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
title_full_unstemmed 4-(Furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
title_sort 4-(furan-2-carbonyl)piperazin-1-ium 3,5-dinitrobenzoate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2014-06-01
description In the cation of the title salt, C9H13N2O2+·C7H3N2O6−, the piperazine ring adopts a slightly distorted chair conformation. Twofold rotational disorder is exhibited by the furan ring in a 0.430 (4):0.570 (4) ratio. In the crystal, N—H...O hydrogen bonds link the ions into chains along [010]. Additional weak C—H...O interactions are observed, leading to a supramolecular layer parallel to (011).
url http://scripts.iucr.org/cgi-bin/paper?S160053681401126X
work_keys_str_mv AT channappankavitha 4furan2carbonylpiperazin1ium35dinitrobenzoate
AT manpreetkaur 4furan2carbonylpiperazin1ium35dinitrobenzoate
AT jerrypjasinski 4furan2carbonylpiperazin1ium35dinitrobenzoate
AT rayjbutcher 4furan2carbonylpiperazin1ium35dinitrobenzoate
AT hsyathirajan 4furan2carbonylpiperazin1ium35dinitrobenzoate
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