Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

The title compound, C21H26N2O5, was unexpectedly obtained as a by-product in the reaction of ethyl acetoacetate, 4-acetamidobenzaldehyde and urea under microwave irradiation. The dihydropyridine ring assumes a flattened boat conformation. Intermolecular N—H...O and weak C&#8212...

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Bibliographic Details
Main Authors: Yiliang Zhao, David E. Hibbs, Paul W. Groundwater, Abram Wassef
Format: Article
Language:English
Published: International Union of Crystallography 2012-08-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S160053681202750X
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spelling doaj-472e36171ff647cf9af11835232137982020-11-25T00:59:44ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-08-01688o2536o253610.1107/S160053681202750XDiethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylateYiliang ZhaoDavid E. HibbsPaul W. GroundwaterAbram WassefThe title compound, C21H26N2O5, was unexpectedly obtained as a by-product in the reaction of ethyl acetoacetate, 4-acetamidobenzaldehyde and urea under microwave irradiation. The dihydropyridine ring assumes a flattened boat conformation. Intermolecular N—H...O and weak C—H...O hydrogen bonding occurs in the crystal.http://scripts.iucr.org/cgi-bin/paper?S160053681202750X
collection DOAJ
language English
format Article
sources DOAJ
author Yiliang Zhao
David E. Hibbs
Paul W. Groundwater
Abram Wassef
spellingShingle Yiliang Zhao
David E. Hibbs
Paul W. Groundwater
Abram Wassef
Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
Acta Crystallographica Section E
author_facet Yiliang Zhao
David E. Hibbs
Paul W. Groundwater
Abram Wassef
author_sort Yiliang Zhao
title Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
title_short Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
title_full Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
title_fullStr Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
title_full_unstemmed Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
title_sort diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-08-01
description The title compound, C21H26N2O5, was unexpectedly obtained as a by-product in the reaction of ethyl acetoacetate, 4-acetamidobenzaldehyde and urea under microwave irradiation. The dihydropyridine ring assumes a flattened boat conformation. Intermolecular N—H...O and weak C—H...O hydrogen bonding occurs in the crystal.
url http://scripts.iucr.org/cgi-bin/paper?S160053681202750X
work_keys_str_mv AT yiliangzhao diethyl44acetamidophenyl26dimethyl14dihydropyridine35dicarboxylate
AT davidehibbs diethyl44acetamidophenyl26dimethyl14dihydropyridine35dicarboxylate
AT paulwgroundwater diethyl44acetamidophenyl26dimethyl14dihydropyridine35dicarboxylate
AT abramwassef diethyl44acetamidophenyl26dimethyl14dihydropyridine35dicarboxylate
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