The influence of pH, temperature and hydrolyzate concentration on the removal of volatile and nonvolatile compounds from sugarcane bagasse hemicellulosic hydrolyzate treated with activated charcoal before or after vacuum evaporation

• Main Authors: R.C.L.B. Rodrigues, M.G.A. Felipe, J.B.Almeida e Silva, M. Vitolo, P.V. Gómez
• Format: Article
• Language: English
• Published: Brazilian Society of Chemical Engineering 2001-09-01
• Series: Brazilian Journal of Chemical Engineering
• Subjects: Sugarcane bagasse; hemicellulosic hydrolyzate; vacuum evaporation; activated charcoal; acetic acid; phenolic compounds
• Online Access: http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322001000300009

This paper analyzes the influence of pH, temperature and degree of hydrolyzate concentration on the removal of volatile and nonvolatile compounds from sugarcane bagasse hemicellulosic hydrolyzate treated with activated charcoal before or after the vacuum evaporation process. Furfural and 5-Hydroxymethylfurfural were almost totally removed in all the experiments, irrespective of pH and temperature and whether the charcoal was added before or after the vacuum evaporation process. Adding activated charcoal before the vacuum evaporation process favored the removal of phenolic compounds for all values of pH. Acetic acid, on the contrary, was most effectively removed when the activated charcoal was added after the vacuum evaporation process at an acid pH (0.92) and at the highest degree of hydrolyzate concentration (f=4). However, addition of activated charcoal before or after vacuum evaporation at an acid pH (0.92) and at the highest degree of hydrolyzate concentration (f=4) favored the removal of both acetic acid and phenolic compounds.