Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate

Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate

The title solvated ester, C22H29NO3S·0.5C6H14, crystallizes with two independent molecules along with a hexane molecule in the asymmetric unit. The two aromatic rings are separated by an –CH2–S– linkage; the rings are aligned at 83.27&#8...

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Main Authors: Azhar Ariffin, Nordiana Nordin, Wagee A. Yehye, Seik Weng Ng
Format: Article
Language:English
Published: International Union of Crystallography 2012-06-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812018739
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spelling doaj-4ff36dbc7d824b538caafb9d8779bef92020-11-24T22:09:34ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-06-01686o1605o160510.1107/S1600536812018739Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvateAzhar AriffinNordiana NordinWagee A. YehyeSeik Weng NgThe title solvated ester, C22H29NO3S·0.5C6H14, crystallizes with two independent molecules along with a hexane molecule in the asymmetric unit. The two aromatic rings are separated by an –CH2–S– linkage; the rings are aligned at 83.27 (4)° in one molecule and 47.66 (7)° in the other. The hydroxy group of one molecule forms an O—H...O hydrogen bond to the other molecule.http://scripts.iucr.org/cgi-bin/paper?S1600536812018739
collection DOAJ
language English
format Article
sources DOAJ
author Azhar Ariffin
Nordiana Nordin
Wagee A. Yehye
Seik Weng Ng
spellingShingle Azhar Ariffin
Nordiana Nordin
Wagee A. Yehye
Seik Weng Ng
Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
Acta Crystallographica Section E
author_facet Azhar Ariffin
Nordiana Nordin
Wagee A. Yehye
Seik Weng Ng
author_sort Azhar Ariffin
title Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
title_short Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
title_full Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
title_fullStr Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
title_full_unstemmed Methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
title_sort methyl 2-[(3,5-di-tert-butyl-4-hydroxybenzyl)sulfanyl]pyridine-3-carboxylate n-hexane hemisolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-06-01
description The title solvated ester, C22H29NO3S·0.5C6H14, crystallizes with two independent molecules along with a hexane molecule in the asymmetric unit. The two aromatic rings are separated by an –CH2–S– linkage; the rings are aligned at 83.27 (4)° in one molecule and 47.66 (7)° in the other. The hydroxy group of one molecule forms an O—H...O hydrogen bond to the other molecule.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812018739
work_keys_str_mv AT azharariffin methyl235ditertbutyl4hydroxybenzylsulfanylpyridine3carboxylatenhexanehemisolvate
AT nordiananordin methyl235ditertbutyl4hydroxybenzylsulfanylpyridine3carboxylatenhexanehemisolvate
AT wageeayehye methyl235ditertbutyl4hydroxybenzylsulfanylpyridine3carboxylatenhexanehemisolvate
AT seikwengng methyl235ditertbutyl4hydroxybenzylsulfanylpyridine3carboxylatenhexanehemisolvate
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