Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance

We report the results from the measurements of high purity Nb samples and superconducting radio-frequency (SRF) cavities doped with nitrogen and followed by either electropolishing (EP) or buffered chemical polishing (BCP), in order to understand the role of the postdoping treatment on the performan...

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Main Authors: Pashupati Dhakal, Gianluigi Ciovati, Uttar Pudasaini, Santosh Chetri, Shreyas Balachandran, Peter J. Lee
Format: Article
Language:English
Published: American Physical Society 2019-12-01
Series:Physical Review Accelerators and Beams
Online Access:http://doi.org/10.1103/PhysRevAccelBeams.22.122002
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spelling doaj-5203e18f0a1e494eb5d0270b523225402020-11-25T00:10:22ZengAmerican Physical SocietyPhysical Review Accelerators and Beams2469-98882019-12-01221212200210.1103/PhysRevAccelBeams.22.122002Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performancePashupati DhakalGianluigi CiovatiUttar PudasainiSantosh ChetriShreyas BalachandranPeter J. LeeWe report the results from the measurements of high purity Nb samples and superconducting radio-frequency (SRF) cavities doped with nitrogen and followed by either electropolishing (EP) or buffered chemical polishing (BCP), in order to understand the role of the postdoping treatment on the performance of SRF cavities. The samples characterization via scanning electron microscope, x-ray photoelectron spectroscopy and secondary ion mass spectroscopy showed topographical differences on the surface of the samples after EP versus BCP treatment, but similar surface composition. Radio-frequency measurements were done on single cell cavities made from fine-grain and large-grain Nb treated by nitrogen doping followed by BCP and showed that improved Q_{0} in the medium field in both fine-grain and large-grain cavities is possible with BCP postprocessing. However, there are differences between performances of large-grain versus fine-grain cavities after BCP. A cavity made from large-grain Nb showed a larger increase in Q_{0} and a lower quench field compared to cavities made from fine-grain Nb.http://doi.org/10.1103/PhysRevAccelBeams.22.122002
collection DOAJ
language English
format Article
sources DOAJ
author Pashupati Dhakal
Gianluigi Ciovati
Uttar Pudasaini
Santosh Chetri
Shreyas Balachandran
Peter J. Lee
spellingShingle Pashupati Dhakal
Gianluigi Ciovati
Uttar Pudasaini
Santosh Chetri
Shreyas Balachandran
Peter J. Lee
Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
Physical Review Accelerators and Beams
author_facet Pashupati Dhakal
Gianluigi Ciovati
Uttar Pudasaini
Santosh Chetri
Shreyas Balachandran
Peter J. Lee
author_sort Pashupati Dhakal
title Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
title_short Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
title_full Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
title_fullStr Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
title_full_unstemmed Surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
title_sort surface characterization of nitrogen-doped high purity niobium coupons compared with superconducting rf cavity performance
publisher American Physical Society
series Physical Review Accelerators and Beams
issn 2469-9888
publishDate 2019-12-01
description We report the results from the measurements of high purity Nb samples and superconducting radio-frequency (SRF) cavities doped with nitrogen and followed by either electropolishing (EP) or buffered chemical polishing (BCP), in order to understand the role of the postdoping treatment on the performance of SRF cavities. The samples characterization via scanning electron microscope, x-ray photoelectron spectroscopy and secondary ion mass spectroscopy showed topographical differences on the surface of the samples after EP versus BCP treatment, but similar surface composition. Radio-frequency measurements were done on single cell cavities made from fine-grain and large-grain Nb treated by nitrogen doping followed by BCP and showed that improved Q_{0} in the medium field in both fine-grain and large-grain cavities is possible with BCP postprocessing. However, there are differences between performances of large-grain versus fine-grain cavities after BCP. A cavity made from large-grain Nb showed a larger increase in Q_{0} and a lower quench field compared to cavities made from fine-grain Nb.
url http://doi.org/10.1103/PhysRevAccelBeams.22.122002
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