Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films

We have already reported that Fe-Ni films prepared in citric-acid-based plating baths show good soft magnetic properties. In this paper, we investigated the effect of the grain size of the Fe-Ni crystalline phase in the films on magnetic properties, and employed an annealing and a pulse plating meth...

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Main Authors: T. Yanai, K. Azuma, K. Eguchi, Y. Watanabe, T. Ohgai, M. Nakano, H. Fukunaga
Format: Article
Language:English
Published: AIP Publishing LLC 2016-05-01
Series:AIP Advances
Online Access:http://dx.doi.org/10.1063/1.4944076
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spelling doaj-545923b415844f93a5c5db200163dc582020-11-25T00:04:59ZengAIP Publishing LLCAIP Advances2158-32262016-05-0165055923055923-610.1063/1.4944076117691ADVEffects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni filmsT. Yanai0K. Azuma1K. Eguchi2Y. Watanabe3T. Ohgai4M. Nakano5H. Fukunaga6 Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, Japan Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, Japan Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, Japan Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, Japan Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, Japan Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, Japan Nagasaki University, 1-14 Bunkyo-Machi, Nagasaki 852-8521, JapanWe have already reported that Fe-Ni films prepared in citric-acid-based plating baths show good soft magnetic properties. In this paper, we investigated the effect of the grain size of the Fe-Ni crystalline phase in the films on magnetic properties, and employed an annealing and a pulse plating method in order to vary the grain size. The coercivity of the annealed Fe-Ni films at 600 °C shows large value, and good correlation between the grain growth and the coercivity was observed. The pulse plating enables us to reduce the grain size of the as-plated Fe-Ni films compared with the DC plating method, and we realized smooth surface and low coercivity of the Fe-Ni films using the pulse plating method. From these results, we confirmed the importance of the reduction in the grain size, and concluded that a pulse plating is an effective method to improve the good soft magnetic properties for our previously-reported Fe-Ni films.http://dx.doi.org/10.1063/1.4944076
collection DOAJ
language English
format Article
sources DOAJ
author T. Yanai
K. Azuma
K. Eguchi
Y. Watanabe
T. Ohgai
M. Nakano
H. Fukunaga
spellingShingle T. Yanai
K. Azuma
K. Eguchi
Y. Watanabe
T. Ohgai
M. Nakano
H. Fukunaga
Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films
AIP Advances
author_facet T. Yanai
K. Azuma
K. Eguchi
Y. Watanabe
T. Ohgai
M. Nakano
H. Fukunaga
author_sort T. Yanai
title Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films
title_short Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films
title_full Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films
title_fullStr Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films
title_full_unstemmed Effects of annealing and pulse plating on soft magnetic properties of electroplated Fe-Ni films
title_sort effects of annealing and pulse plating on soft magnetic properties of electroplated fe-ni films
publisher AIP Publishing LLC
series AIP Advances
issn 2158-3226
publishDate 2016-05-01
description We have already reported that Fe-Ni films prepared in citric-acid-based plating baths show good soft magnetic properties. In this paper, we investigated the effect of the grain size of the Fe-Ni crystalline phase in the films on magnetic properties, and employed an annealing and a pulse plating method in order to vary the grain size. The coercivity of the annealed Fe-Ni films at 600 °C shows large value, and good correlation between the grain growth and the coercivity was observed. The pulse plating enables us to reduce the grain size of the as-plated Fe-Ni films compared with the DC plating method, and we realized smooth surface and low coercivity of the Fe-Ni films using the pulse plating method. From these results, we confirmed the importance of the reduction in the grain size, and concluded that a pulse plating is an effective method to improve the good soft magnetic properties for our previously-reported Fe-Ni films.
url http://dx.doi.org/10.1063/1.4944076
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