Green synthesis and crystal structure of 3-(benzothiazol-2-yl)thiophene

Green synthesis and crystal structure of 3-(benzothiazol-2-yl)thiophene

The title compound, C11H7NS2, was prepared in high yield (87%) using a solvent-free microwave-assisted synthesis. The structure shows whole-molecule disorder with occupancies for two orientations (A and B) of 0.4884 (10) and 0.5116 (10), respectively. The thiophene and benzothiazole rings are almost...

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Bibliographic Details
Main Authors: Linh Nguyen Ngoc, Trung Vu Quoc, Hoan Duong Quoc, Manh Vu Quoc, Luong Truong Minh, Chien Thang Pham, Luc Van Meervelt
Format: Article
Language:English
Published: International Union of Crystallography 2017-11-01
Series:Acta Crystallographica Section E: Crystallographic Communications
Subjects:
crystal structure
thiophene
benzothiazole
microwave-assisted synthesis
solvent-free
whole-molecule disorder
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2056989017014530

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