Synthesis, characterization and visible light photocatalytic activity of Mg2+ and Zr4+ co-doped TiO2 nanomaterial for degradation of methylene blue

Mg2+ and Zr4+ co-doped TiO2 was synthesized by sol–gel method. Catalysts were characterized by XRD, UV–vis DRS, SEM-EDX, TEM, BET, XPS and FT-IR to evaluate the crystal patterns and crystallite size (5.07–18.9 nm), bandgap energy, morphology, surface area, surface composition with oxidation states a...

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Bibliographic Details
Main Authors: Desta Shumuye Meshesha, Ravi Chandra Matangi, Siva Rao Tirukkovalluri, Sreedhar Bojja
Format: Article
Language:English
Published: Taylor & Francis Group 2017-06-01
Series:Journal of Asian Ceramic Societies
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2187076416301105
Description
Summary:Mg2+ and Zr4+ co-doped TiO2 was synthesized by sol–gel method. Catalysts were characterized by XRD, UV–vis DRS, SEM-EDX, TEM, BET, XPS and FT-IR to evaluate the crystal patterns and crystallite size (5.07–18.9 nm), bandgap energy, morphology, surface area, surface composition with oxidation states and incorporation of dopants into TiO2 lattice. Degradation of methylene blue was carried out under visible light irradiation by varying the reaction parameters such as initial dye concentration, catalyst loading and pH of the solution. 1.0 wt% Mg2+ and 0.25 wt% Zr4+ codoped TiO2 was found to be an efficient catalyst.
ISSN:2187-0764