1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide

1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide

In the crystal structure of the title compound, C11H9ClN4O3, pairs of N—H...N(imidazole) hydrogen bonds connect the molecules into centrosymmetric dimers, which are further connected by N—H...O(carbamoyl) hydrogen bonds into C(4) chains along [010]. Interplay of these two...

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Main Authors: Maciej Kubicki, Paweł Wagner, Artur Korzański
Format: Article
Language:English
Published: International Union of Crystallography 2011-10-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536811036609
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spelling doaj-5e8c285c7b8e483ebfd1c6c825fba1392020-11-25T02:40:30ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-10-016710o2626o262610.1107/S16005368110366091-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamideMaciej KubickiPaweł WagnerArtur KorzańskiIn the crystal structure of the title compound, C11H9ClN4O3, pairs of N—H...N(imidazole) hydrogen bonds connect the molecules into centrosymmetric dimers, which are further connected by N—H...O(carbamoyl) hydrogen bonds into C(4) chains along [010]. Interplay of these two kinds of hydrogen bonds connect the molecules into layers perpendicular to [101]. The imidazole [maximum deviation 0.0069 (9) Å] and phenyl rings are inclined at a dihedral angle of 58.44 (6)°; the nitro group is almost coplanar [dihedral angle 5.8 (2)°] with the imidazole ring while the carbamoyl group is almost perpendicular [70.15 (13)°] to it.http://scripts.iucr.org/cgi-bin/paper?S1600536811036609
collection DOAJ
language English
format Article
sources DOAJ
author Maciej Kubicki
Paweł Wagner
Artur Korzański
spellingShingle Maciej Kubicki
Paweł Wagner
Artur Korzański
1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide
Acta Crystallographica Section E
author_facet Maciej Kubicki
Paweł Wagner
Artur Korzański
author_sort Maciej Kubicki
title 1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide
title_short 1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide
title_full 1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide
title_fullStr 1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide
title_full_unstemmed 1-(3-Chlorophenyl)-2-methyl-4-nitro-1H-imidazole-5-carboxamide
title_sort 1-(3-chlorophenyl)-2-methyl-4-nitro-1h-imidazole-5-carboxamide
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2011-10-01
description In the crystal structure of the title compound, C11H9ClN4O3, pairs of N—H...N(imidazole) hydrogen bonds connect the molecules into centrosymmetric dimers, which are further connected by N—H...O(carbamoyl) hydrogen bonds into C(4) chains along [010]. Interplay of these two kinds of hydrogen bonds connect the molecules into layers perpendicular to [101]. The imidazole [maximum deviation 0.0069 (9) Å] and phenyl rings are inclined at a dihedral angle of 58.44 (6)°; the nitro group is almost coplanar [dihedral angle 5.8 (2)°] with the imidazole ring while the carbamoyl group is almost perpendicular [70.15 (13)°] to it.
url http://scripts.iucr.org/cgi-bin/paper?S1600536811036609
work_keys_str_mv AT maciejkubicki 13chlorophenyl2methyl4nitro1himidazole5carboxamide
AT paweamp322wagner 13chlorophenyl2methyl4nitro1himidazole5carboxamide
AT arturkorzaamp324ski 13chlorophenyl2methyl4nitro1himidazole5carboxamide
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