N-Benzoyl-N′-(2-chloro-3-pyridyl)thiourea

The title compound, C13H10ClN3OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothiocyanate at room temperature. The thiourea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings,...

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Bibliographic Details
Main Authors: Yu-Jie Ding, Jian Yao, Jian-Chao Wu, Wen-Kui Dong, Jun-Feng Tong
Format: Article
Language:English
Published: International Union of Crystallography 2009-08-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809027081
Description
Summary:The title compound, C13H10ClN3OS, was prepared by the reaction of 3-amino-2-chloropyridine with benzoyl isothiocyanate at room temperature. The thiourea group makes dihedral angles of 47.17 (5) and 51.88 (4)°, respectively, with the benzene and pyridyl rings, while the angle between the benzene and pyridine rings is 8.91 (3)°. Intermolecular hydrogen-bond interactions link neighbouring molecules into an infinite supramolecular structure.
ISSN:1600-5368