1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone

1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone

In the title compound, C22H20Cl2N2O, the diazole ring adopts a shallow envelope conformation with the methine C atom bonded to the adjacent chlorobenzene ring as the flap. The dihedral angles between the heterocyclic ring and the pendant chlorobenzene rings are 61.4 (2) and 80.3 (2)°. In the crystal...

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Bibliographic Details
Main Authors: Farook Adam, Nadiah Ameram, Seranthimata Samshuddin, Kurady Akhilesh Bairy, Madhugiri Shivashankarappa Sunil
Format: Article
Language:English
Published: International Union of Crystallography 2016-03-01
Series:IUCrData
Subjects:
crystal structure
indazole derivative
synthesis
C—H...Cl interactions
Online Access:http://scripts.iucr.org/cgi-bin/paper?S2414314616004740
id doaj-73343e475719451c9a871a0188a0bffb
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spelling doaj-73343e475719451c9a871a0188a0bffb2020-11-24T21:37:02ZengInternational Union of CrystallographyIUCrData2414-31462016-03-0113x16047410.1107/S2414314616004740hb40291-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanoneFarook Adam0Nadiah Ameram1Seranthimata Samshuddin2Kurady Akhilesh Bairy3Madhugiri Shivashankarappa Sunil4School of Chemical Sciences, Unibersiti Science Malaysia, 11800, Minden, Pulau Pinang., MalaysiaSchool of Chemical Sciences, Universiti Science Malaysia, 11800, Minden, Pulau Pinang., MalaysiaDepartment of P.G. Studies in Chemistry, Alva's College, Moodbidri, Karnataka 574 227, IndiaDepartment of Chemistry, SDM Institute of Technology, Ujire, Karnataka 574 240, IndiaDepartment of Chemistry, SDM Institute of Technology, Ujire, Karnataka 574 240, IndiaIn the title compound, C22H20Cl2N2O, the diazole ring adopts a shallow envelope conformation with the methine C atom bonded to the adjacent chlorobenzene ring as the flap. The dihedral angles between the heterocyclic ring and the pendant chlorobenzene rings are 61.4 (2) and 80.3 (2)°. In the crystal, weak C—H...Cl interactions connect the molecules into [001] chains.http://scripts.iucr.org/cgi-bin/paper?S2414314616004740crystal structureindazole derivativesynthesisC—H...Cl interactions
collection DOAJ
language English
format Article
sources DOAJ
author Farook Adam
Nadiah Ameram
Seranthimata Samshuddin
Kurady Akhilesh Bairy
Madhugiri Shivashankarappa Sunil
spellingShingle Farook Adam
Nadiah Ameram
Seranthimata Samshuddin
Kurady Akhilesh Bairy
Madhugiri Shivashankarappa Sunil
1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone
IUCrData
crystal structure
indazole derivative
synthesis
C—H...Cl interactions
author_facet Farook Adam
Nadiah Ameram
Seranthimata Samshuddin
Kurady Akhilesh Bairy
Madhugiri Shivashankarappa Sunil
author_sort Farook Adam
title 1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone
title_short 1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone
title_full 1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone
title_fullStr 1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone
title_full_unstemmed 1-[(7E)-7-(2-Chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazol-2-yl]ethanone
title_sort 1-[(7e)-7-(2-chlorobenzylidene)-3-(2-chlorophenyl)-3,3a,4,5,6,7-hexahydro-2h-indazol-2-yl]ethanone
publisher International Union of Crystallography
series IUCrData
issn 2414-3146
publishDate 2016-03-01
description In the title compound, C22H20Cl2N2O, the diazole ring adopts a shallow envelope conformation with the methine C atom bonded to the adjacent chlorobenzene ring as the flap. The dihedral angles between the heterocyclic ring and the pendant chlorobenzene rings are 61.4 (2) and 80.3 (2)°. In the crystal, weak C—H...Cl interactions connect the molecules into [001] chains.
topic crystal structure
indazole derivative
synthesis
C—H...Cl interactions
url http://scripts.iucr.org/cgi-bin/paper?S2414314616004740
work_keys_str_mv AT farookadam 17e72chlorobenzylidene32chlorophenyl33a4567hexahydro2hindazol2ylethanone
AT nadiahameram 17e72chlorobenzylidene32chlorophenyl33a4567hexahydro2hindazol2ylethanone
AT seranthimatasamshuddin 17e72chlorobenzylidene32chlorophenyl33a4567hexahydro2hindazol2ylethanone
AT kuradyakhileshbairy 17e72chlorobenzylidene32chlorophenyl33a4567hexahydro2hindazol2ylethanone
AT madhugirishivashankarappasunil 17e72chlorobenzylidene32chlorophenyl33a4567hexahydro2hindazol2ylethanone
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