Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V

We present the modification of Ti-6Al-4V surfaces with a diode end-pumped Nd:YVO4 laser by varying the distance between laser-produced micro(μ)-channels. We analyzed the influence of laser texturing on the morphology, microstructure, surface and corrosion properties of Ti-6Al-4V. SEM imaging reveals...

Full description

Bibliographic Details
Main Authors: Marjetka Conradi, Aleksandra Kocijan, Damjan Klobčar, Matjaž Godec
Format: Article
Language:English
Published: MDPI AG 2020-11-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/10/11/1504
id doaj-7727b17105ea4526b79332dbe702d28e
record_format Article
spelling doaj-7727b17105ea4526b79332dbe702d28e2020-11-25T04:04:39ZengMDPI AGMetals2075-47012020-11-01101504150410.3390/met10111504Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4VMarjetka Conradi0Aleksandra Kocijan1Damjan Klobčar2Matjaž Godec3Institute of Metals and Technology, Lepi pot 11, 1000 Ljubljana, SloveniaInstitute of Metals and Technology, Lepi pot 11, 1000 Ljubljana, SloveniaFaculty of Mechanical Engineering, University of Ljubljana, Aškerčeva 6, 1000 Ljubljana, SloveniaInstitute of Metals and Technology, Lepi pot 11, 1000 Ljubljana, SloveniaWe present the modification of Ti-6Al-4V surfaces with a diode end-pumped Nd:YVO4 laser by varying the distance between laser-produced micro(μ)-channels. We analyzed the influence of laser texturing on the morphology, microstructure, surface and corrosion properties of Ti-6Al-4V. SEM imaging reveals a characteristic μ-channel pattern with different scan line separations, while electron backscatter diffraction (EBSD) indicates that laser texturing with the current parameters influences the microstructure up to 2 µm deep with the most significant influence at the tips, where melting and rapid solidification occur. The Vickers hardness test indicates a surface hardening effect of the laser-textured compared to the as-received Ti-6Al-4V surfaces. The XPS analysis showed that the oxide layer on the laser-textured samples was considerably thicker compared to the as-received sample, at 20 and 7 nm, respectively. We observed that the wettability was strongly correlated with the scan line separation. The results show increased hydrophobicity with increased scan line separation. The corrosion resistance was improved for laser-textured surfaces compared to the as-received surface and increased with the scan line separation.https://www.mdpi.com/2075-4701/10/11/1504surface textureTi-6Al-4V alloymicrostructurewettabilitycorrosion
collection DOAJ
language English
format Article
sources DOAJ
author Marjetka Conradi
Aleksandra Kocijan
Damjan Klobčar
Matjaž Godec
spellingShingle Marjetka Conradi
Aleksandra Kocijan
Damjan Klobčar
Matjaž Godec
Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V
Metals
surface texture
Ti-6Al-4V alloy
microstructure
wettability
corrosion
author_facet Marjetka Conradi
Aleksandra Kocijan
Damjan Klobčar
Matjaž Godec
author_sort Marjetka Conradi
title Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V
title_short Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V
title_full Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V
title_fullStr Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V
title_full_unstemmed Influence of Laser Texturing on Microstructure, Surface and Corrosion Properties of Ti-6Al-4V
title_sort influence of laser texturing on microstructure, surface and corrosion properties of ti-6al-4v
publisher MDPI AG
series Metals
issn 2075-4701
publishDate 2020-11-01
description We present the modification of Ti-6Al-4V surfaces with a diode end-pumped Nd:YVO4 laser by varying the distance between laser-produced micro(μ)-channels. We analyzed the influence of laser texturing on the morphology, microstructure, surface and corrosion properties of Ti-6Al-4V. SEM imaging reveals a characteristic μ-channel pattern with different scan line separations, while electron backscatter diffraction (EBSD) indicates that laser texturing with the current parameters influences the microstructure up to 2 µm deep with the most significant influence at the tips, where melting and rapid solidification occur. The Vickers hardness test indicates a surface hardening effect of the laser-textured compared to the as-received Ti-6Al-4V surfaces. The XPS analysis showed that the oxide layer on the laser-textured samples was considerably thicker compared to the as-received sample, at 20 and 7 nm, respectively. We observed that the wettability was strongly correlated with the scan line separation. The results show increased hydrophobicity with increased scan line separation. The corrosion resistance was improved for laser-textured surfaces compared to the as-received surface and increased with the scan line separation.
topic surface texture
Ti-6Al-4V alloy
microstructure
wettability
corrosion
url https://www.mdpi.com/2075-4701/10/11/1504
work_keys_str_mv AT marjetkaconradi influenceoflasertexturingonmicrostructuresurfaceandcorrosionpropertiesofti6al4v
AT aleksandrakocijan influenceoflasertexturingonmicrostructuresurfaceandcorrosionpropertiesofti6al4v
AT damjanklobcar influenceoflasertexturingonmicrostructuresurfaceandcorrosionpropertiesofti6al4v
AT matjazgodec influenceoflasertexturingonmicrostructuresurfaceandcorrosionpropertiesofti6al4v
_version_ 1724435819685478400