A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
A novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions. This fluorous organocatalyst could be recovered and recycled several times with good purity....
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2017-02-01
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Online Access: | http://www.mdpi.com/2073-4344/7/2/66 |
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doaj-836e56f5e5474887baaafc341ce4f7fc2020-11-25T00:19:42ZengMDPI AGCatalysts2073-43442017-02-01726610.3390/catal7020066catal7020066A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐ChlorosuccinimideYi‐Wei Zhu0Yi‐Xin Shi1Yu‐Qi Yin2School of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, ChinaSchool of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, ChinaSchool of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, ChinaA novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions. This fluorous organocatalyst could be recovered and recycled several times with good purity.http://www.mdpi.com/2073-4344/7/2/66organocatalysisꞵ‐chloroethers recycle fluorous solid‐phase extraction (F‐SPE) |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Yi‐Wei Zhu Yi‐Xin Shi Yu‐Qi Yin |
spellingShingle |
Yi‐Wei Zhu Yi‐Xin Shi Yu‐Qi Yin A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide Catalysts organocatalysis ꞵ‐chloroethers recycle fluorous solid‐phase extraction (F‐SPE) |
author_facet |
Yi‐Wei Zhu Yi‐Xin Shi Yu‐Qi Yin |
author_sort |
Yi‐Wei Zhu |
title |
A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide |
title_short |
A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide |
title_full |
A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide |
title_fullStr |
A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide |
title_full_unstemmed |
A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide |
title_sort |
recyclable fluorous hydrazine‐1,2bis(carbothioate) organocatalyst for the synthesis of ꞵ‐chloroethers with n‐chlorosuccinimide |
publisher |
MDPI AG |
series |
Catalysts |
issn |
2073-4344 |
publishDate |
2017-02-01 |
description |
A novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions. This fluorous organocatalyst could be recovered and recycled several times with good purity. |
topic |
organocatalysis ꞵ‐chloroethers recycle fluorous solid‐phase extraction (F‐SPE) |
url |
http://www.mdpi.com/2073-4344/7/2/66 |
work_keys_str_mv |
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1725370565002264576 |