A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide

A novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic  activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions.  This  fluorous  organocatalyst  could  be  recovered  and  recycled  several  times  with   good purity....

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Main Authors: Yi‐Wei Zhu, Yi‐Xin Shi, Yu‐Qi Yin
Format: Article
Language:English
Published: MDPI AG 2017-02-01
Series:Catalysts
Subjects:
Online Access:http://www.mdpi.com/2073-4344/7/2/66
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spelling doaj-836e56f5e5474887baaafc341ce4f7fc2020-11-25T00:19:42ZengMDPI AGCatalysts2073-43442017-02-01726610.3390/catal7020066catal7020066A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐ChlorosuccinimideYi‐Wei Zhu0Yi‐Xin Shi1Yu‐Qi Yin2School of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, ChinaSchool of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, ChinaSchool of Biology and Chemical Engineering, Anhui Polytechnic University, 8 Middle Beijing Road, Wuhu 241000, Anhui, ChinaA novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic  activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions.  This  fluorous  organocatalyst  could  be  recovered  and  recycled  several  times  with   good purity.http://www.mdpi.com/2073-4344/7/2/66organocatalysisꞵ‐chloroethers recycle fluorous solid‐phase extraction (F‐SPE)
collection DOAJ
language English
format Article
sources DOAJ
author Yi‐Wei Zhu
Yi‐Xin Shi
Yu‐Qi Yin
spellingShingle Yi‐Wei Zhu
Yi‐Xin Shi
Yu‐Qi Yin
A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
Catalysts
organocatalysis
ꞵ‐chloroethers
 recycle
 fluorous solid‐phase extraction (F‐SPE)
author_facet Yi‐Wei Zhu
Yi‐Xin Shi
Yu‐Qi Yin
author_sort Yi‐Wei Zhu
title A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
title_short A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
title_full A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
title_fullStr A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
title_full_unstemmed A Recyclable Fluorous Hydrazine‐1,2Bis(Carbothioate) Organocatalyst for the Synthesis of ꞵ‐Chloroethers with N‐Chlorosuccinimide
title_sort recyclable fluorous hydrazine‐1,2bis(carbothioate) organocatalyst for the synthesis of ꞵ‐chloroethers with n‐chlorosuccinimide
publisher MDPI AG
series Catalysts
issn 2073-4344
publishDate 2017-02-01
description A novel fluorous hydrazine‐1,2‐bis(carbothioate) was prepared. It showed good catalytic  activity in the synthesis of ꞵ‐chloroethers with N‐chlorosuccinimide under mild reaction conditions.  This  fluorous  organocatalyst  could  be  recovered  and  recycled  several  times  with   good purity.
topic organocatalysis
ꞵ‐chloroethers
 recycle
 fluorous solid‐phase extraction (F‐SPE)
url http://www.mdpi.com/2073-4344/7/2/66
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