Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]

Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]

In the title compound, C38H32F2N4O4S, the ethyl chain of the ethoxycarbonyl group displays rotational disorder with site occupancy factors ca 0.6 and 0.4. The S atom lies on a twofold rotation axis. There are both inter- and intramolecular hydrogen bonds in the crystal structure. An intramolecular N...

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Main Authors: Ming Li, Guo-Rui Cao, Li-Rong Weng
Format: Article
Language:English
Published: International Union of Crystallography 2008-01-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536807061545
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spelling doaj-84f1f7fd6fd248f98679f0cdc2f6784e2020-11-25T00:54:57ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682008-01-01641o21o2110.1107/S1600536807061545Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]Ming LiGuo-Rui CaoLi-Rong WengIn the title compound, C38H32F2N4O4S, the ethyl chain of the ethoxycarbonyl group displays rotational disorder with site occupancy factors ca 0.6 and 0.4. The S atom lies on a twofold rotation axis. There are both inter- and intramolecular hydrogen bonds in the crystal structure. An intramolecular N—H...O hydrogen bond forms a six-membered ring, while an intermolecular N—H...F hydrogen bond results in a chain.http://scripts.iucr.org/cgi-bin/paper?S1600536807061545
collection DOAJ
language English
format Article
sources DOAJ
author Ming Li
Guo-Rui Cao
Li-Rong Weng
spellingShingle Ming Li
Guo-Rui Cao
Li-Rong Weng
Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]
Acta Crystallographica Section E
author_facet Ming Li
Guo-Rui Cao
Li-Rong Weng
author_sort Ming Li
title Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]
title_short Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]
title_full Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]
title_fullStr Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]
title_full_unstemmed Diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1H-pyrrole-3-carboxylate]
title_sort diethyl 5,5′-thiobis[2-amino-4-(4-fluorophenyl)-1-phenyl-1h-pyrrole-3-carboxylate]
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2008-01-01
description In the title compound, C38H32F2N4O4S, the ethyl chain of the ethoxycarbonyl group displays rotational disorder with site occupancy factors ca 0.6 and 0.4. The S atom lies on a twofold rotation axis. There are both inter- and intramolecular hydrogen bonds in the crystal structure. An intramolecular N—H...O hydrogen bond forms a six-membered ring, while an intermolecular N—H...F hydrogen bond results in a chain.
url http://scripts.iucr.org/cgi-bin/paper?S1600536807061545
work_keys_str_mv AT mingli diethyl558242thiobis2amino44fluorophenyl1phenyl1hpyrrole3carboxylate
AT guoruicao diethyl558242thiobis2amino44fluorophenyl1phenyl1hpyrrole3carboxylate
AT lirongweng diethyl558242thiobis2amino44fluorophenyl1phenyl1hpyrrole3carboxylate
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