9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione
In the title compound, C33H27BrClNO4, the dihydropyridine ring adopts a flattened boat conformation. The molecular conformation is stabilized by an intramolecular O—H...O hydrogen bond, with an S(8) ring motif. In the crystal, O—H...O, C—H...O and C—H...Cl hydrogen bonds, and C—H...π interactions li...
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International Union of Crystallography
2014-06-01
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Series: | Acta Crystallographica Section E |
Online Access: | http://scripts.iucr.org/cgi-bin/paper?S1600536814010460 |
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doaj-88177d54ff8f43fca5620bbd9d0fd9db2020-11-25T02:34:34ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682014-06-01706o663o66410.1107/S1600536814010460hg53959-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dioneMehmet Akkurt0Shaaban K. Mohamed1Antar A. Abdelhamid2Abdel-Aal M. Gaber3Mustafa R. Albayati4Department of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, TurkeyChemistry and Environmental Division, Manchester Metropolitan University, Manchester M1 5GD, EnglandChemistry Department, Faculty of Science, Sohag University, 82524 Sohag, EgyptDepartment of Chemistry, Faculty of Science, Assiut University, 71516 Assiut, EgyptKirkuk University, College of Science, Department of Chemistry, Kirkuk, IraqIn the title compound, C33H27BrClNO4, the dihydropyridine ring adopts a flattened boat conformation. The molecular conformation is stabilized by an intramolecular O—H...O hydrogen bond, with an S(8) ring motif. In the crystal, O—H...O, C—H...O and C—H...Cl hydrogen bonds, and C—H...π interactions link the molecules, forming a three-dimensional network. In the acridinedione ring system, the two ring C atoms at the 2- and 3-positions, and the C atom at the 6-position and the atoms of the phenyl ring attached to the C atom at the 6-position are disordered over two sets of sites with occupancy ratios of 0.783 (5):0.217 (5) and 0.526 (18):0.474 (18), respectively.http://scripts.iucr.org/cgi-bin/paper?S1600536814010460 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Mehmet Akkurt Shaaban K. Mohamed Antar A. Abdelhamid Abdel-Aal M. Gaber Mustafa R. Albayati |
spellingShingle |
Mehmet Akkurt Shaaban K. Mohamed Antar A. Abdelhamid Abdel-Aal M. Gaber Mustafa R. Albayati 9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione Acta Crystallographica Section E |
author_facet |
Mehmet Akkurt Shaaban K. Mohamed Antar A. Abdelhamid Abdel-Aal M. Gaber Mustafa R. Albayati |
author_sort |
Mehmet Akkurt |
title |
9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione |
title_short |
9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione |
title_full |
9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione |
title_fullStr |
9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione |
title_full_unstemmed |
9-(3-Bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2H,5H)-dione |
title_sort |
9-(3-bromo-5-chloro-2-hydroxyphenyl)-10-(2-hydroxyethyl)-3,6-diphenyl-3,4,9,10-tetrahydroacridine-1,8(2h,5h)-dione |
publisher |
International Union of Crystallography |
series |
Acta Crystallographica Section E |
issn |
1600-5368 |
publishDate |
2014-06-01 |
description |
In the title compound, C33H27BrClNO4, the dihydropyridine ring adopts a flattened boat conformation. The molecular conformation is stabilized by an intramolecular O—H...O hydrogen bond, with an S(8) ring motif. In the crystal, O—H...O, C—H...O and C—H...Cl hydrogen bonds, and C—H...π interactions link the molecules, forming a three-dimensional network. In the acridinedione ring system, the two ring C atoms at the 2- and 3-positions, and the C atom at the 6-position and the atoms of the phenyl ring attached to the C atom at the 6-position are disordered over two sets of sites with occupancy ratios of 0.783 (5):0.217 (5) and 0.526 (18):0.474 (18), respectively. |
url |
http://scripts.iucr.org/cgi-bin/paper?S1600536814010460 |
work_keys_str_mv |
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1724808077503365120 |