The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven
A series of beta-amino esters alpha,beta-unsaturated ketones and esters 4a-h and 6a-d derived from alpha-amino acids have been prepared starting from alpha-amino esters hydrochorides 2a-d with 1,3- dicarbonyl compounds 3a,b and 5 in presence of triethylamine. These compounds have been prepared under...
Main Authors: | , , , , |
---|---|
Format: | Article |
Language: | English |
Published: |
Sociedade Brasileira de Química
2006-01-01
|
Series: | Journal of the Brazilian Chemical Society |
Subjects: | |
Online Access: | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000100026 |
id |
doaj-8f28ac2a00ef432bb571e12d4ba2a5f0 |
---|---|
record_format |
Article |
spelling |
doaj-8f28ac2a00ef432bb571e12d4ba2a5f02020-11-25T02:13:56ZengSociedade Brasileira de QuímicaJournal of the Brazilian Chemical Society0103-50531678-47902006-01-01171184188The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave ovenBraibante Mara E. F.Braibante Hugo T. S.Morel Ademir F.Costa Carla C.Lima Marcelo G.A series of beta-amino esters alpha,beta-unsaturated ketones and esters 4a-h and 6a-d derived from alpha-amino acids have been prepared starting from alpha-amino esters hydrochorides 2a-d with 1,3- dicarbonyl compounds 3a,b and 5 in presence of triethylamine. These compounds have been prepared under domestic microwave oven, under solvent free condition with and without solid support (K-10 or KSF).http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000100026alpha-amino acidssolid supportmicrowavealpha-amino esters |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Braibante Mara E. F. Braibante Hugo T. S. Morel Ademir F. Costa Carla C. Lima Marcelo G. |
spellingShingle |
Braibante Mara E. F. Braibante Hugo T. S. Morel Ademir F. Costa Carla C. Lima Marcelo G. The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven Journal of the Brazilian Chemical Society alpha-amino acids solid support microwave alpha-amino esters |
author_facet |
Braibante Mara E. F. Braibante Hugo T. S. Morel Ademir F. Costa Carla C. Lima Marcelo G. |
author_sort |
Braibante Mara E. F. |
title |
The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven |
title_short |
The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven |
title_full |
The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven |
title_fullStr |
The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven |
title_full_unstemmed |
The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven |
title_sort |
solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven |
publisher |
Sociedade Brasileira de Química |
series |
Journal of the Brazilian Chemical Society |
issn |
0103-5053 1678-4790 |
publishDate |
2006-01-01 |
description |
A series of beta-amino esters alpha,beta-unsaturated ketones and esters 4a-h and 6a-d derived from alpha-amino acids have been prepared starting from alpha-amino esters hydrochorides 2a-d with 1,3- dicarbonyl compounds 3a,b and 5 in presence of triethylamine. These compounds have been prepared under domestic microwave oven, under solvent free condition with and without solid support (K-10 or KSF). |
topic |
alpha-amino acids solid support microwave alpha-amino esters |
url |
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532006000100026 |
work_keys_str_mv |
AT braibantemaraef thesolventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT braibantehugots thesolventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT morelademirf thesolventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT costacarlac thesolventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT limamarcelog thesolventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT braibantemaraef solventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT braibantehugots solventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT morelademirf solventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT costacarlac solventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven AT limamarcelog solventfreepreparationofbetaaminoestersalphabetaunsaturatedketonesandesterswithdomesticmicrowaveoven |
_version_ |
1724903196323741696 |