3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate

3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate

In the title compound, C38H42N4O4·C2H6O, prepared via a spirolactam ring-formation reaction in a rhodamine dye, the xanthene ring system is approximately planar (r.m.s. deviation = 0.0014Å) and subtends dihedral angles of 88.10 (3) and 86.92 (4)&...

Full description

Bibliographic Details
Main Authors: Xujun Zheng, Jinlong Guo, Zhen Wei, Qun Wan, Shunwei Chen
Format: Article
Language:English
Published: International Union of Crystallography 2012-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536812016741
id doaj-95adb9a9fd6d48e5b1a3a0344ec34df9
record_format Article
spelling doaj-95adb9a9fd6d48e5b1a3a0344ec34df92020-11-25T01:27:46ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682012-05-01685o1479o147910.1107/S16005368120167413′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvateXujun ZhengJinlong GuoZhen WeiQun WanShunwei ChenIn the title compound, C38H42N4O4·C2H6O, prepared via a spirolactam ring-formation reaction in a rhodamine dye, the xanthene ring system is approximately planar (r.m.s. deviation = 0.0014Å) and subtends dihedral angles of 88.10 (3) and 86.92 (4)° with the spirolactam (r.m.s. deviations = 0.0012 Å) and benzene rings, respectively. The crystal structure consists of chains parallel to [-101], formed via O—H...O interactions.http://scripts.iucr.org/cgi-bin/paper?S1600536812016741
collection DOAJ
language English
format Article
sources DOAJ
author Xujun Zheng
Jinlong Guo
Zhen Wei
Qun Wan
Shunwei Chen
spellingShingle Xujun Zheng
Jinlong Guo
Zhen Wei
Qun Wan
Shunwei Chen
3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
Acta Crystallographica Section E
author_facet Xujun Zheng
Jinlong Guo
Zhen Wei
Qun Wan
Shunwei Chen
author_sort Xujun Zheng
title 3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
title_short 3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
title_full 3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
title_fullStr 3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
title_full_unstemmed 3′,6′-Bis(diethylamino)-2-[(E)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
title_sort 3′,6′-bis(diethylamino)-2-[(e)-2-(4-hydroxy-3-methoxybenzylideneamino)ethyl]spiro[isoindoline-1,9′-xanthen]-3-one ethanol monosolvate
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2012-05-01
description In the title compound, C38H42N4O4·C2H6O, prepared via a spirolactam ring-formation reaction in a rhodamine dye, the xanthene ring system is approximately planar (r.m.s. deviation = 0.0014Å) and subtends dihedral angles of 88.10 (3) and 86.92 (4)° with the spirolactam (r.m.s. deviations = 0.0012 Å) and benzene rings, respectively. The crystal structure consists of chains parallel to [-101], formed via O—H...O interactions.
url http://scripts.iucr.org/cgi-bin/paper?S1600536812016741
work_keys_str_mv AT xujunzheng 3amp82426amp8242bisdiethylamino2e24hydroxy3methoxybenzylideneaminoethylspiroisoindoline19amp8242xanthen3oneethanolmonosolvate
AT jinlongguo 3amp82426amp8242bisdiethylamino2e24hydroxy3methoxybenzylideneaminoethylspiroisoindoline19amp8242xanthen3oneethanolmonosolvate
AT zhenwei 3amp82426amp8242bisdiethylamino2e24hydroxy3methoxybenzylideneaminoethylspiroisoindoline19amp8242xanthen3oneethanolmonosolvate
AT qunwan 3amp82426amp8242bisdiethylamino2e24hydroxy3methoxybenzylideneaminoethylspiroisoindoline19amp8242xanthen3oneethanolmonosolvate
AT shunweichen 3amp82426amp8242bisdiethylamino2e24hydroxy3methoxybenzylideneaminoethylspiroisoindoline19amp8242xanthen3oneethanolmonosolvate
_version_ 1725103373135380480

Similar Items