Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides
Some new macrocyclic dibenzotetraoxadiamides, tribenzotetraoxadimides, tribenzopentaoxadiamide, tribenzohexaoxadiamide, and tetrabenzoheptaoxadiamide 15-22 have been prepared. These compounds were obtained in the macrocyclization step by reacting the diamines 6 and 7 with appropriate dicarboxylic ac...
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Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR
2000-06-01
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doaj-9b154698443a4fc59137707b70cfde482020-11-25T03:31:53ZengIranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECRIranian Journal of Chemistry & Chemical Engineering 1021-99861021-99862000-06-0119161210199Efficient Synthesis of a Range of Benzosubstituted Macrocyclic DiamidesHashem Sharghi0Ahmad Reza Massah1Khodabakhsh Niknam2Department of Chemistry, Shiraz University, Zip code 71454, Shiraz, I.R. IRANDepartment of Chemistry, Shiraz University, Zip code 71454, Shiraz, I.R. IRANDepartment of Chemistry, Shiraz University, Zip code 71454, Shiraz, I.R. IRANSome new macrocyclic dibenzotetraoxadiamides, tribenzotetraoxadimides, tribenzopentaoxadiamide, tribenzohexaoxadiamide, and tetrabenzoheptaoxadiamide 15-22 have been prepared. These compounds were obtained in the macrocyclization step by reacting the diamines 6 and 7 with appropriate dicarboxylic acid dichlorides 8-14. The cyclization does not require high dilution techniques or template effect and provides the expected dilactams in high yields ranging from 63% to 81%.http://www.ijcce.ac.ir/article_10199_3f0816a9e5003cff873ee9a0e8775719.pdfmacrocyclic diamidessynthesisdirect macrocyclizationdicarboxylic acid dichloride |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Hashem Sharghi Ahmad Reza Massah Khodabakhsh Niknam |
spellingShingle |
Hashem Sharghi Ahmad Reza Massah Khodabakhsh Niknam Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides Iranian Journal of Chemistry & Chemical Engineering macrocyclic diamides synthesis direct macrocyclization dicarboxylic acid dichloride |
author_facet |
Hashem Sharghi Ahmad Reza Massah Khodabakhsh Niknam |
author_sort |
Hashem Sharghi |
title |
Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides |
title_short |
Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides |
title_full |
Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides |
title_fullStr |
Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides |
title_full_unstemmed |
Efficient Synthesis of a Range of Benzosubstituted Macrocyclic Diamides |
title_sort |
efficient synthesis of a range of benzosubstituted macrocyclic diamides |
publisher |
Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR |
series |
Iranian Journal of Chemistry & Chemical Engineering |
issn |
1021-9986 1021-9986 |
publishDate |
2000-06-01 |
description |
Some new macrocyclic dibenzotetraoxadiamides, tribenzotetraoxadimides, tribenzopentaoxadiamide, tribenzohexaoxadiamide, and tetrabenzoheptaoxadiamide 15-22 have been prepared. These compounds were obtained in the macrocyclization step by reacting the diamines 6 and 7 with appropriate dicarboxylic acid dichlorides 8-14. The cyclization does not require high dilution techniques or template effect and provides the expected dilactams in high yields ranging from 63% to 81%. |
topic |
macrocyclic diamides synthesis direct macrocyclization dicarboxylic acid dichloride |
url |
http://www.ijcce.ac.ir/article_10199_3f0816a9e5003cff873ee9a0e8775719.pdf |
work_keys_str_mv |
AT hashemsharghi efficientsynthesisofarangeofbenzosubstitutedmacrocyclicdiamides AT ahmadrezamassah efficientsynthesisofarangeofbenzosubstitutedmacrocyclicdiamides AT khodabakhshniknam efficientsynthesisofarangeofbenzosubstitutedmacrocyclicdiamides |
_version_ |
1724571001549750272 |