Experimental and simulation analysis of residual topography dominated deformation mechanism of nanoindentation: a case study of Inconel 625 superalloy

• Main Authors: Kaidi Li, Jinshan Li, Bin Tang, William Yi Wang, Fulong Chen, Mengqi Zhang, Jiangkun Fan, Hong Zhong
• Format: Article
• Language: English
• Published: Elsevier 2021-07-01
• Series: Journal of Materials Research and Technology
• Subjects: Residual topography; Nanoindentation; Superalloys; Crystal plasticity finite element method; Schmid factors
• Online Access: http://www.sciencedirect.com/science/article/pii/S2238785421004944

The microscopic deformation behavior of Inconel 625 superalloy has been investigated by means of nanoindentation experiments and crystal plasticity finite element simulations. Based on the electron backscattered diffraction characterizations, the nanoindentation simulations were performed on grains with various orientations. The simulated load–displacement curves match well with those of experiment and the maximum difference in materials hardness between the experimental and the simulation result is about 6.86%, which is within the accuracy of the model. Moreover, surface Schmid factor (SSF) and interior Schmid factor (ISF) were proposed out and the scanning electron microscope and atomic force microscope characterizations were carried out. The results show that the pile-up tends to occur at the locations with a large SSF. Subsequently, the simulations of nanoindentation on [001]-, [011]-, and [111]-oriented grains were performed by the established model. It is revealed that the residual topography changes periodically when the indenter is fixed and the crystal only rotates around the Z-axis of the sample coordinate system. Combining with the analysis of the ISF, this periodicity of residual topography reflects the superimposed effect of the slip systems, and a large ISF promotes the in-plane displacement of the interior material which inhibiting the evolution of pile-up, while a small ISF leads to a high pile-up.