Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines
The grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives in the presence of 30 mol% of acetic acid to give 3,1-benzoxazines are described. The reactions were performed at room temperature affording 3,1-benzoxazines in yields above 95% and high purity when benzaldehyde and...
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Chemical Society of Ethiopia
2014-05-01
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| Series: | Bulletin of the Chemical Society of Ethiopia |
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| Online Access: | http://www.ajol.info/index.php/bcse/article/view/103692 |
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doaj-9e0e27bd8c29437fb5ac4b100458d83a2020-11-25T01:13:21ZengChemical Society of EthiopiaBulletin of the Chemical Society of Ethiopia1011-39241726-801X2014-05-0128230130410.4314/bcse.v28i2.14Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazinesI. B. MasesaneE. MuriithiT. H. TabaneThe grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives in the presence of 30 mol% of acetic acid to give 3,1-benzoxazines are described. The reactions were performed at room temperature affording 3,1-benzoxazines in yields above 95% and high purity when benzaldehyde and its chloro and nitro derivatives were used. DOI: http://dx.doi.org/10.4314/bcse.v28i2.14http://www.ajol.info/index.php/bcse/article/view/1036922-Aminobenzyl alcoholBenzaldehydeAcetic acid31-Benzoxazines |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
I. B. Masesane E. Muriithi T. H. Tabane |
| spellingShingle |
I. B. Masesane E. Muriithi T. H. Tabane Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines Bulletin of the Chemical Society of Ethiopia 2-Aminobenzyl alcohol Benzaldehyde Acetic acid 3 1-Benzoxazines |
| author_facet |
I. B. Masesane E. Muriithi T. H. Tabane |
| author_sort |
I. B. Masesane |
| title |
Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines |
| title_short |
Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines |
| title_full |
Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines |
| title_fullStr |
Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines |
| title_full_unstemmed |
Simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines |
| title_sort |
simple grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives, a rapid synthetic route to 3,1-benzoxazines |
| publisher |
Chemical Society of Ethiopia |
| series |
Bulletin of the Chemical Society of Ethiopia |
| issn |
1011-3924 1726-801X |
| publishDate |
2014-05-01 |
| description |
The grinding-induced reactions of 2-aminobenzyl alcohol and benzaldehyde derivatives in the presence of 30 mol% of acetic acid to give 3,1-benzoxazines are described. The reactions were performed at room temperature affording 3,1-benzoxazines in yields above 95% and high purity when benzaldehyde and its chloro and nitro derivatives were used. DOI: http://dx.doi.org/10.4314/bcse.v28i2.14 |
| topic |
2-Aminobenzyl alcohol Benzaldehyde Acetic acid 3 1-Benzoxazines |
| url |
http://www.ajol.info/index.php/bcse/article/view/103692 |
| work_keys_str_mv |
AT ibmasesane simplegrindinginducedreactionsof2aminobenzylalcoholandbenzaldehydederivativesarapidsyntheticrouteto31benzoxazines AT emuriithi simplegrindinginducedreactionsof2aminobenzylalcoholandbenzaldehydederivativesarapidsyntheticrouteto31benzoxazines AT thtabane simplegrindinginducedreactionsof2aminobenzylalcoholandbenzaldehydederivativesarapidsyntheticrouteto31benzoxazines |
| _version_ |
1725162963730432000 |