The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives

Zeolite Y clay modified copper nitrate catalyst was prepared. The obtained catalyst was analyzed by SEM, EDS, and powder XRD techniques. The zeolite Y clay modified copper nitrate catalyst was used for the synthesis of various substituted mesalazine by sulfonylation. The synthesized sulfonamides hav...

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Main Authors:	Dineshkumar Selvakumar, Thirunarayanan Ganesamoorthi, Mayavel Perumal, Muthuvel Inbasekaran
Format:	Article
Language:	English
Published:	Sciendo 2016-06-01
Series:	Analele Universităţii "Ovidius" Constanţa: Seria Chimie
Subjects:	sulfonamides copper-zeolites ft-ir nmr spectra gc-mass sem eds powder xrd
Online Access:	https://doi.org/10.1515/auoc-2016-0005

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spelling	doaj-9f0695862c294f508deb522c9e26bd642021-09-06T19:40:17ZengSciendoAnalele Universităţii "Ovidius" Constanţa: Seria Chimie2286-038X2016-06-01271222710.1515/auoc-2016-0005auoc-2016-0005The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivativesDineshkumar Selvakumar0Thirunarayanan Ganesamoorthi1Mayavel Perumal2Muthuvel Inbasekaran3Department of Chemistry, Annamalai University, Annamaliangar-608002, Tamilnadu, IndiaDepartment of Chemistry, Annamalai University, Annamaliangar-608002, Tamilnadu, IndiaDepartment of Chemistry, Annamalai University, Annamaliangar-608002, Tamilnadu, IndiaDepartment of Chemistry, Annamalai University, Annamaliangar-608002, Tamilnadu, IndiaZeolite Y clay modified copper nitrate catalyst was prepared. The obtained catalyst was analyzed by SEM, EDS, and powder XRD techniques. The zeolite Y clay modified copper nitrate catalyst was used for the synthesis of various substituted mesalazine by sulfonylation. The synthesized sulfonamides have been characterized by GC-MS, IR, 1H, 13C and HSQC NMR techniques. The yield percentages of sulfonamides are more than 85%.https://doi.org/10.1515/auoc-2016-0005sulfonamidescopper-zeolitesft-irnmr spectragc-masssemedspowder xrd
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Dineshkumar Selvakumar Thirunarayanan Ganesamoorthi Mayavel Perumal Muthuvel Inbasekaran
spellingShingle	Dineshkumar Selvakumar Thirunarayanan Ganesamoorthi Mayavel Perumal Muthuvel Inbasekaran The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives Analele Universităţii "Ovidius" Constanţa: Seria Chimie sulfonamides copper-zeolites ft-ir nmr spectra gc-mass sem eds powder xrd
author_facet	Dineshkumar Selvakumar Thirunarayanan Ganesamoorthi Mayavel Perumal Muthuvel Inbasekaran
author_sort	Dineshkumar Selvakumar
title	The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives
title_short	The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives
title_full	The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives
title_fullStr	The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives
title_full_unstemmed	The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives
title_sort	utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives
publisher	Sciendo
series	Analele Universităţii "Ovidius" Constanţa: Seria Chimie
issn	2286-038X
publishDate	2016-06-01
description	Zeolite Y clay modified copper nitrate catalyst was prepared. The obtained catalyst was analyzed by SEM, EDS, and powder XRD techniques. The zeolite Y clay modified copper nitrate catalyst was used for the synthesis of various substituted mesalazine by sulfonylation. The synthesized sulfonamides have been characterized by GC-MS, IR, 1H, 13C and HSQC NMR techniques. The yield percentages of sulfonamides are more than 85%.
topic	sulfonamides copper-zeolites ft-ir nmr spectra gc-mass sem eds powder xrd
url	https://doi.org/10.1515/auoc-2016-0005
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The utilization of copper/zeolite as catalyst in the microwave-assisted synthesis of some novel sulfonamide derivatives

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