2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one

2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one

The title compound, C20H16N2O4S, was prepared by introduction of a 2-nitrobenzyl group to 2-(furan-2-yl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one via an alkaline-catalysed reaction. The thiazepine ring adopts a twist-boat conformation. The furan ring is oriented at dihedral angles of 56.75&#...

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Bibliographic Details
Main Authors: De-Yong Ye, Yong Chu, Zhao-Hui Huang
Format: Article
Language:English
Published: International Union of Crystallography 2011-01-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536810052098
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spelling doaj-a2354c6d91dc45b0bd157899c71d9ed02020-11-25T02:31:25ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682011-01-01671o168o16810.1107/S16005368100520982-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-oneDe-Yong YeYong ChuZhao-Hui HuangThe title compound, C20H16N2O4S, was prepared by introduction of a 2-nitrobenzyl group to 2-(furan-2-yl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one via an alkaline-catalysed reaction. The thiazepine ring adopts a twist-boat conformation. The furan ring is oriented at dihedral angles of 56.75 (14) and 10.82 (14)° with respect to the two benzene rings, while the two benzene rings make a dihedral angle of 62.96 (10)°. Weak intermolecular C—H...O hydrogen bonds occur in the crystal structure. http://scripts.iucr.org/cgi-bin/paper?S1600536810052098
collection DOAJ
language English
format Article
sources DOAJ
author De-Yong Ye
Yong Chu
Zhao-Hui Huang
spellingShingle De-Yong Ye
Yong Chu
Zhao-Hui Huang
2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
Acta Crystallographica Section E
author_facet De-Yong Ye
Yong Chu
Zhao-Hui Huang
author_sort De-Yong Ye
title 2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
title_short 2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
title_full 2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
title_fullStr 2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
title_full_unstemmed 2-(Furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
title_sort 2-(furan-2-yl)-5-(2-nitrobenzyl)-2,3-dihydro-1,5-benzothiazepin-4(5h)-one
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2011-01-01
description The title compound, C20H16N2O4S, was prepared by introduction of a 2-nitrobenzyl group to 2-(furan-2-yl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one via an alkaline-catalysed reaction. The thiazepine ring adopts a twist-boat conformation. The furan ring is oriented at dihedral angles of 56.75 (14) and 10.82 (14)° with respect to the two benzene rings, while the two benzene rings make a dihedral angle of 62.96 (10)°. Weak intermolecular C—H...O hydrogen bonds occur in the crystal structure.
url http://scripts.iucr.org/cgi-bin/paper?S1600536810052098
work_keys_str_mv AT deyongye 2furan2yl52nitrobenzyl23dihydro15benzothiazepin45hone
AT yongchu 2furan2yl52nitrobenzyl23dihydro15benzothiazepin45hone
AT zhaohuihuang 2furan2yl52nitrobenzyl23dihydro15benzothiazepin45hone
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