Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid
We synthesized Pd-Fe series nanoparticles in solid solution using pulsed plasma in liquid with Pd-Fe bulk mixture electrodes. The Pd-Fe atomic percent ratios were 1:3, 1:1, and 3:1, and the particle size was measured to be less than 10 nm by high-resolution transmission electron microscopy (HR-TEM)....
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MDPI AG
2018-12-01
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| Series: | Nanomaterials |
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| Online Access: | https://www.mdpi.com/2079-4991/8/12/1068 |
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doaj-adea862a01e54505acc29a5a8c6e8e7b2020-11-24T23:41:10ZengMDPI AGNanomaterials2079-49912018-12-01812106810.3390/nano8121068nano8121068Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in LiquidShota Tamura0Tsutomu Mashimo1Kenta Yamamoto2Zhazgul Kelgenbaeva3Weijan Ma4Xuesong Kang5Michio Koinuma6Hiroshi Isobe7Akira Yoshiasa8Institute of Pulsed Power Science, Kumamoto University, Kumamoto 860-0862, JapanInstitute of Pulsed Power Science, Kumamoto University, Kumamoto 860-0862, JapanInstitute of Pulsed Power Science, Kumamoto University, Kumamoto 860-0862, JapanInstitute of Pulsed Power Science, Kumamoto University, Kumamoto 860-0862, JapanInstitute of Pulsed Power Science, Kumamoto University, Kumamoto 860-0862, JapanInstitute of Pulsed Power Science, Kumamoto University, Kumamoto 860-0862, JapanFaculty of Engineering, Kumamoto University, Kumamoto 860-0862, JapanFaculty of Science, Kumamoto University, Kumamoto 860-0862, JapanFaculty of Science, Kumamoto University, Kumamoto 860-0862, JapanWe synthesized Pd-Fe series nanoparticles in solid solution using pulsed plasma in liquid with Pd-Fe bulk mixture electrodes. The Pd-Fe atomic percent ratios were 1:3, 1:1, and 3:1, and the particle size was measured to be less than 10 nm by high-resolution transmission electron microscopy (HR-TEM). The nanoparticles showed face-centered cubic structure. The lattice parameter increased with increasing Pd content and followed Vegard’s law, and energy-dispersive X-ray spectra were consistent with the ratios of the starting samples, which showed a solid solution state. The solid solution structure and local structure were confirmed by HR-TEM and X-ray absorption fine structure.https://www.mdpi.com/2079-4991/8/12/1068Pd-Fe alloynanoparticlepulsed plasma in liquid |
| collection |
DOAJ |
| language |
English |
| format |
Article |
| sources |
DOAJ |
| author |
Shota Tamura Tsutomu Mashimo Kenta Yamamoto Zhazgul Kelgenbaeva Weijan Ma Xuesong Kang Michio Koinuma Hiroshi Isobe Akira Yoshiasa |
| spellingShingle |
Shota Tamura Tsutomu Mashimo Kenta Yamamoto Zhazgul Kelgenbaeva Weijan Ma Xuesong Kang Michio Koinuma Hiroshi Isobe Akira Yoshiasa Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid Nanomaterials Pd-Fe alloy nanoparticle pulsed plasma in liquid |
| author_facet |
Shota Tamura Tsutomu Mashimo Kenta Yamamoto Zhazgul Kelgenbaeva Weijan Ma Xuesong Kang Michio Koinuma Hiroshi Isobe Akira Yoshiasa |
| author_sort |
Shota Tamura |
| title |
Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid |
| title_short |
Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid |
| title_full |
Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid |
| title_fullStr |
Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid |
| title_full_unstemmed |
Synthesis of Pd-Fe System Alloy Nanoparticles by Pulsed Plasma in Liquid |
| title_sort |
synthesis of pd-fe system alloy nanoparticles by pulsed plasma in liquid |
| publisher |
MDPI AG |
| series |
Nanomaterials |
| issn |
2079-4991 |
| publishDate |
2018-12-01 |
| description |
We synthesized Pd-Fe series nanoparticles in solid solution using pulsed plasma in liquid with Pd-Fe bulk mixture electrodes. The Pd-Fe atomic percent ratios were 1:3, 1:1, and 3:1, and the particle size was measured to be less than 10 nm by high-resolution transmission electron microscopy (HR-TEM). The nanoparticles showed face-centered cubic structure. The lattice parameter increased with increasing Pd content and followed Vegard’s law, and energy-dispersive X-ray spectra were consistent with the ratios of the starting samples, which showed a solid solution state. The solid solution structure and local structure were confirmed by HR-TEM and X-ray absorption fine structure. |
| topic |
Pd-Fe alloy nanoparticle pulsed plasma in liquid |
| url |
https://www.mdpi.com/2079-4991/8/12/1068 |
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