(S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one

(S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one

The title compound, C19H27NO3, was obtained by the reaction of (3S,7aR)-7a-hexyl-7-methoxy-3-phenyl-2,3-dihydropyrrolo[2,1-b]oxazol-5(7aH)-one and triethylsilane using titanium(IV) chloride as catalyst. In the molecule, the phenyl and dihydropyrrolone rings form a dihedral angle of 83.8&#819...

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Main Authors: Jian-Nan Guo, Li-Jiao Jiang, Jian-Feng Zheng
Format: Article
Language:English
Published: International Union of Crystallography 2009-05-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809014160
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spelling doaj-b0b364a2ec4b470ca6bf88adb906529f2020-11-25T00:54:22ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-05-01655o1094o109410.1107/S1600536809014160(S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-oneJian-Nan GuoLi-Jiao JiangJian-Feng ZhengThe title compound, C19H27NO3, was obtained by the reaction of (3S,7aR)-7a-hexyl-7-methoxy-3-phenyl-2,3-dihydropyrrolo[2,1-b]oxazol-5(7aH)-one and triethylsilane using titanium(IV) chloride as catalyst. In the molecule, the phenyl and dihydropyrrolone rings form a dihedral angle of 83.8 (1)°. O—H...O hydrogen-bonding interactions lead to the formation of a chain parallel to the a axis. http://scripts.iucr.org/cgi-bin/paper?S1600536809014160
collection DOAJ
language English
format Article
sources DOAJ
author Jian-Nan Guo
Li-Jiao Jiang
Jian-Feng Zheng
spellingShingle Jian-Nan Guo
Li-Jiao Jiang
Jian-Feng Zheng
(S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one
Acta Crystallographica Section E
author_facet Jian-Nan Guo
Li-Jiao Jiang
Jian-Feng Zheng
author_sort Jian-Nan Guo
title (S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one
title_short (S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one
title_full (S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one
title_fullStr (S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one
title_full_unstemmed (S)-5-Hexyl-1-[(S)-2-hydroxy-1-phenylethyl]-4-methoxy-1H-pyrrol-2(5H)-one
title_sort (s)-5-hexyl-1-[(s)-2-hydroxy-1-phenylethyl]-4-methoxy-1h-pyrrol-2(5h)-one
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-05-01
description The title compound, C19H27NO3, was obtained by the reaction of (3S,7aR)-7a-hexyl-7-methoxy-3-phenyl-2,3-dihydropyrrolo[2,1-b]oxazol-5(7aH)-one and triethylsilane using titanium(IV) chloride as catalyst. In the molecule, the phenyl and dihydropyrrolone rings form a dihedral angle of 83.8 (1)°. O—H...O hydrogen-bonding interactions lead to the formation of a chain parallel to the a axis.
url http://scripts.iucr.org/cgi-bin/paper?S1600536809014160
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AT lijiaojiang s5hexyl1s2hydroxy1phenylethyl4methoxy1hpyrrol25hone
AT jianfengzheng s5hexyl1s2hydroxy1phenylethyl4methoxy1hpyrrol25hone
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