Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process
This study investigated a new potential hot-pressing method for wood modification, in which densification, drying, and heat-treatment were carried out in sequence. The effects of heat treatment on the chemical components of wood were evaluated. The specimens were treated at different temperatures (1...
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North Carolina State University
2016-03-01
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doaj-b0b90c18c36040f48ac14eacc79b08042020-11-24T21:52:42ZengNorth Carolina State UniversityBioResources1930-21261930-21262016-03-011123856387410.15376/biores.11.2.3856-3874Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing ProcessLili Li0Ximing Wang1Feiyu Wu2Inner Mongolia Agricultural University; ChinaInner Mongolia Agricultural University; ChinaInner Mongolia Agricultural University; ChinaThis study investigated a new potential hot-pressing method for wood modification, in which densification, drying, and heat-treatment were carried out in sequence. The effects of heat treatment on the chemical components of wood were evaluated. The specimens were treated at different temperatures (180 to 220 °C) for 2 to 5 h. Holocellulose, α-cellulose, and lignin were extracted from the treated and untreated milled wood. The changes in these components were analyzed by thermogravimetry (TG) and Fourier-transform infrared spectroscopy (FTIR). Due to its amorphous structure, most hemicelluloses were degraded when it was exposed to 220 °C for 3 h and to 200 °C for 5 h. Conversely, the lignin contents increased continuously throughout the treatment due to the loss of polysaccharides and the formation of cross-links. Because of the crystallinity, α-cellulose degradation was slight. According to the analysis of functional groups, FTIR showed treated wood was more hydrophobic than the untreated one.http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_2_3856_Li_Chemical_Analysis_Densification_Drying_Heat-TreatmentHot-pressingHeat treatmentChemical changes |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Lili Li Ximing Wang Feiyu Wu |
spellingShingle |
Lili Li Ximing Wang Feiyu Wu Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process BioResources Hot-pressing Heat treatment Chemical changes |
author_facet |
Lili Li Ximing Wang Feiyu Wu |
author_sort |
Lili Li |
title |
Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process |
title_short |
Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process |
title_full |
Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process |
title_fullStr |
Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process |
title_full_unstemmed |
Chemical Analysis of Densification, Drying, and Heat Treatment of Scots pine (Pinus sylvestris L.) through a Hot-Pressing Process |
title_sort |
chemical analysis of densification, drying, and heat treatment of scots pine (pinus sylvestris l.) through a hot-pressing process |
publisher |
North Carolina State University |
series |
BioResources |
issn |
1930-2126 1930-2126 |
publishDate |
2016-03-01 |
description |
This study investigated a new potential hot-pressing method for wood modification, in which densification, drying, and heat-treatment were carried out in sequence. The effects of heat treatment on the chemical components of wood were evaluated. The specimens were treated at different temperatures (180 to 220 °C) for 2 to 5 h. Holocellulose, α-cellulose, and lignin were extracted from the treated and untreated milled wood. The changes in these components were analyzed by thermogravimetry (TG) and Fourier-transform infrared spectroscopy (FTIR). Due to its amorphous structure, most hemicelluloses were degraded when it was exposed to 220 °C for 3 h and to 200 °C for 5 h. Conversely, the lignin contents increased continuously throughout the treatment due to the loss of polysaccharides and the formation of cross-links. Because of the crystallinity, α-cellulose degradation was slight. According to the analysis of functional groups, FTIR showed treated wood was more hydrophobic than the untreated one. |
topic |
Hot-pressing Heat treatment Chemical changes |
url |
http://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_11_2_3856_Li_Chemical_Analysis_Densification_Drying_Heat-Treatment |
work_keys_str_mv |
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