Syntheses of Stable Isotope Labeled D12-Malachite Green

Syntheses of Stable Isotope Labeled D12-Malachite Green

The efficient synthesis of stable isotope labeled D12-Malachite Green with CD3OD as the precursor by methylation, condensation and oxidation was presented. The yields of D12-Malachite Green was 50.1 % based on CD3OD consumed. The product was ideatified by HPLC, MS, and NMR to be the target compound...

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Main Author: YANG Chao;YANG Wei-cheng;LI Mei-hua;LUO Yong
Format: Article
Language:zho
Published: Editorial Board of Journal of Isotopes 2014-02-01
Series:Journal of Isotopes
Subjects:
isotope labeled Malachite Green synthesis characterization
Online Access:http://www.tws.org.cn/CN/10.7538/tws.2014.27.02.0077
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spelling doaj-bc434f6f85044d94b7b7a2797b1c747d2020-11-24T21:43:51ZzhoEditorial Board of Journal of IsotopesJournal of Isotopes1000-75121000-75122014-02-01272778110.7538/tws.2014.27.02.0077 Syntheses of Stable Isotope Labeled D12-Malachite GreenYANG Chao;YANG Wei-cheng;LI Mei-hua;LUO YongThe efficient synthesis of stable isotope labeled D12-Malachite Green with CD3OD as the precursor by methylation, condensation and oxidation was presented. The yields of D12-Malachite Green was 50.1 % based on CD3OD consumed. The product was ideatified by HPLC, MS, and NMR to be the target compound. Its chemical purity and isotopic enrichment were higher than 99.0 atom%D. The result showed that the D12-Malachite Green could be used as internal standard in the field of food safety. http://www.tws.org.cn/CN/10.7538/tws.2014.27.02.0077 isotope labeled Malachite Green synthesis characterization
collection DOAJ
language zho
format Article
sources DOAJ
author YANG Chao;YANG Wei-cheng;LI Mei-hua;LUO Yong
spellingShingle YANG Chao;YANG Wei-cheng;LI Mei-hua;LUO Yong
Syntheses of Stable Isotope Labeled D12-Malachite Green
Journal of Isotopes
isotope labeled Malachite Green synthesis characterization
author_facet YANG Chao;YANG Wei-cheng;LI Mei-hua;LUO Yong
author_sort YANG Chao;YANG Wei-cheng;LI Mei-hua;LUO Yong
title Syntheses of Stable Isotope Labeled D12-Malachite Green
title_short Syntheses of Stable Isotope Labeled D12-Malachite Green
title_full Syntheses of Stable Isotope Labeled D12-Malachite Green
title_fullStr Syntheses of Stable Isotope Labeled D12-Malachite Green
title_full_unstemmed Syntheses of Stable Isotope Labeled D12-Malachite Green
title_sort syntheses of stable isotope labeled d12-malachite green
publisher Editorial Board of Journal of Isotopes
series Journal of Isotopes
issn 1000-7512
1000-7512
publishDate 2014-02-01
description The efficient synthesis of stable isotope labeled D12-Malachite Green with CD3OD as the precursor by methylation, condensation and oxidation was presented. The yields of D12-Malachite Green was 50.1 % based on CD3OD consumed. The product was ideatified by HPLC, MS, and NMR to be the target compound. Its chemical purity and isotopic enrichment were higher than 99.0 atom%D. The result showed that the D12-Malachite Green could be used as internal standard in the field of food safety.
topic isotope labeled Malachite Green synthesis characterization
url http://www.tws.org.cn/CN/10.7538/tws.2014.27.02.0077
work_keys_str_mv AT yangchaoyangweichenglimeihualuoyong synthesesofstableisotopelabeledd12malachitegreen
_version_ 1725911702579445760

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