Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube

The effects of heat treatment on the microstructure, mechanical properties and electrochemical property of the as-extruded Mg-5Zn-1Mn (ZM51) alloy tube are investigated by optical microstructure (OM), X-ray diffractometer (XRD), scanning electron microscopy (SEM), transmission electrical microscope...

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Main Authors: Lianhui Li, Hongshuai Cao, Fugang Qi, Qing Wang, Nie Zhao, Yingdu Liu, Xue Ye, Xiaoping Ouyang
Format: Article
Language:English
Published: MDPI AG 2020-02-01
Series:Metals
Subjects:
Online Access:https://www.mdpi.com/2075-4701/10/3/301
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spelling doaj-c11b39c9c6b14d3a89fe0a3e59bfa3422020-11-25T02:16:18ZengMDPI AGMetals2075-47012020-02-0110330110.3390/met10030301met10030301Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy TubeLianhui Li0Hongshuai Cao1Fugang Qi2Qing Wang3Nie Zhao4Yingdu Liu5Xue Ye6Xiaoping Ouyang7School of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaSchool of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaSchool of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaChina Railway Eryuan Engineering Group Co. Ltd., Chengdu 610000, ChinaSchool of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaSchool of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaSchool of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaSchool of Materials Science and Engineering, Xiangtan University, Xiangtan 411105, ChinaThe effects of heat treatment on the microstructure, mechanical properties and electrochemical property of the as-extruded Mg-5Zn-1Mn (ZM51) alloy tube are investigated by optical microstructure (OM), X-ray diffractometer (XRD), scanning electron microscopy (SEM), transmission electrical microscope (TEM), uniaxial tensile test, and electrochemical test. The results show that the as-cast structure is a typical dendritic structure, mainly composed of &#945;-Mg and Mg<sub>7</sub>Zn<sub>3</sub> eutectic compounds. After homogenization, most of Mg<sub>7</sub>Zn<sub>3</sub> eutectic phases are dissolved in the Mg matrix. During the extrusion process, the ZM51 alloy has undergone complete dynamic recrystallization and has a good elongation, reaching 21.4%. T6, especially T4 + double aging treatment, can significantly improve the mechanical properties of the as-extruded tube. The microstructure reveals that the precipitation strengthening of the finely dispersed MgZn<sub>2 </sub>precipitates is the main reason for the strength increase. The fracture micromorphology of the as-extruded tube is mainly composed of dimples and cleavage facets, which is a typical ductile fracture. The fracture mode of the as-aged alloy tubes belongs to cleavage fracture. In addition, the electrochemical test results show the solution-treated ZM51 alloy tube has the best corrosion resistance. The improvement of corrosion resistance is mainly due to the microstructure uniformity and low phase volume fraction.https://www.mdpi.com/2075-4701/10/3/301extruded tubeheat treatmentmechanical propertiescorrosion resistance
collection DOAJ
language English
format Article
sources DOAJ
author Lianhui Li
Hongshuai Cao
Fugang Qi
Qing Wang
Nie Zhao
Yingdu Liu
Xue Ye
Xiaoping Ouyang
spellingShingle Lianhui Li
Hongshuai Cao
Fugang Qi
Qing Wang
Nie Zhao
Yingdu Liu
Xue Ye
Xiaoping Ouyang
Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube
Metals
extruded tube
heat treatment
mechanical properties
corrosion resistance
author_facet Lianhui Li
Hongshuai Cao
Fugang Qi
Qing Wang
Nie Zhao
Yingdu Liu
Xue Ye
Xiaoping Ouyang
author_sort Lianhui Li
title Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube
title_short Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube
title_full Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube
title_fullStr Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube
title_full_unstemmed Effect of Heat Treatment on Microstructure and Mechanical Properties of Mg-5Zn-1Mn Alloy Tube
title_sort effect of heat treatment on microstructure and mechanical properties of mg-5zn-1mn alloy tube
publisher MDPI AG
series Metals
issn 2075-4701
publishDate 2020-02-01
description The effects of heat treatment on the microstructure, mechanical properties and electrochemical property of the as-extruded Mg-5Zn-1Mn (ZM51) alloy tube are investigated by optical microstructure (OM), X-ray diffractometer (XRD), scanning electron microscopy (SEM), transmission electrical microscope (TEM), uniaxial tensile test, and electrochemical test. The results show that the as-cast structure is a typical dendritic structure, mainly composed of &#945;-Mg and Mg<sub>7</sub>Zn<sub>3</sub> eutectic compounds. After homogenization, most of Mg<sub>7</sub>Zn<sub>3</sub> eutectic phases are dissolved in the Mg matrix. During the extrusion process, the ZM51 alloy has undergone complete dynamic recrystallization and has a good elongation, reaching 21.4%. T6, especially T4 + double aging treatment, can significantly improve the mechanical properties of the as-extruded tube. The microstructure reveals that the precipitation strengthening of the finely dispersed MgZn<sub>2 </sub>precipitates is the main reason for the strength increase. The fracture micromorphology of the as-extruded tube is mainly composed of dimples and cleavage facets, which is a typical ductile fracture. The fracture mode of the as-aged alloy tubes belongs to cleavage fracture. In addition, the electrochemical test results show the solution-treated ZM51 alloy tube has the best corrosion resistance. The improvement of corrosion resistance is mainly due to the microstructure uniformity and low phase volume fraction.
topic extruded tube
heat treatment
mechanical properties
corrosion resistance
url https://www.mdpi.com/2075-4701/10/3/301
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