2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol

2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol

The title compound, C21H24Br2N2O3, was synthesized by the condensation reaction of 3-methoxysalicylaldehyde with 4-(2-amino-3,5-dibromobenzylamino)cyclohexanol in a methanol solution. The dihedral angle between the two benzene rings is 76.4 (3)°. The cyclohexyl ring adopts...

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Format: Article
Language:English
Published: International Union of Crystallography 2009-03-01
Series:Acta Crystallographica Section E
Online Access:http://scripts.iucr.org/cgi-bin/paper?S1600536809005182
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spelling doaj-c39dbd71fe4645fdae8127c0a15207022020-11-25T02:13:59ZengInternational Union of CrystallographyActa Crystallographica Section E1600-53682009-03-01653o550o55010.1107/S16005368090051822-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenolThe title compound, C21H24Br2N2O3, was synthesized by the condensation reaction of 3-methoxysalicylaldehyde with 4-(2-amino-3,5-dibromobenzylamino)cyclohexanol in a methanol solution. The dihedral angle between the two benzene rings is 76.4 (3)°. The cyclohexyl ring adopts a chair configuration. There is an intramolecular O—H...N hydrogen bond which affects the solid state conformation of the molecule. The crystal structure is stabilized by intermolecular O—H...O hydrogen bonds, forming chains running along the b axis. http://scripts.iucr.org/cgi-bin/paper?S1600536809005182
collection DOAJ
language English
format Article
sources DOAJ
title 2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
spellingShingle 2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
Acta Crystallographica Section E
title_short 2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
title_full 2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
title_fullStr 2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
title_full_unstemmed 2-[6,8-Dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
title_sort 2-[6,8-dibromo-3-(4-hydroxycyclohexyl)-1,2,3,4-tetrahydroquinazolin-2-yl]-6-methoxyphenol
publisher International Union of Crystallography
series Acta Crystallographica Section E
issn 1600-5368
publishDate 2009-03-01
description The title compound, C21H24Br2N2O3, was synthesized by the condensation reaction of 3-methoxysalicylaldehyde with 4-(2-amino-3,5-dibromobenzylamino)cyclohexanol in a methanol solution. The dihedral angle between the two benzene rings is 76.4 (3)°. The cyclohexyl ring adopts a chair configuration. There is an intramolecular O—H...N hydrogen bond which affects the solid state conformation of the molecule. The crystal structure is stabilized by intermolecular O—H...O hydrogen bonds, forming chains running along the b axis.
url http://scripts.iucr.org/cgi-bin/paper?S1600536809005182
_version_ 1724902752537018368

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