1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone

In the title compound, C24H22N4O2S, the dihedral angle between the triazole and thiophene rings is 4.83 (14)°. The dihedral angles between the triazole and tolyl rings and between the thiophene and phenyl rings are 48.42 (16) and 9.23 (13)°, respectively. An intramolecular N—H...O hydrogen bond clos...

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Main Authors:	Gamal A. El-Hiti, Bakr F. Abdel-Wahab, Rizk E. Khidre, Mohamed S. Mostafa, Amany S. Hegazy, Benson M. Kariuki
Format:	Article
Language:	English
Published:	International Union of Crystallography 2018-03-01
Series:	IUCrData
Subjects:	crystal structure 1,2,3-triazole thiophene
Online Access:	http://scripts.iucr.org/cgi-bin/paper?S2414314618004029

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spelling	doaj-c523ecdc121f42fcab8db47fcce332512020-11-25T01:06:08ZengInternational Union of CrystallographyIUCrData2414-31462018-03-0133x18040210.1107/S2414314618004029hb42141-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanoneGamal A. El-Hiti0Bakr F. Abdel-Wahab1Rizk E. Khidre2Mohamed S. Mostafa3Amany S. Hegazy4Benson M. Kariuki5Cornea Research Chair, Department of Optometry, College of Applied Medical Sciences, King Saud University, PO Box 10219, Riyadh 11433, Saudi ArabiaDepartment of Chemistry, College of Science and Humanities, Shaqra University, Duwadimi, Saudi ArabiaChemistry Department, Faculty of Science, Jazan University, Jazan 2079, Saudi ArabiaChemistry Department, Faculty of Science, Damietta University, EgyptSchool of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10 3AT, UKSchool of Chemistry, Cardiff University, Main Building, Park Place, Cardiff CF10 3AT, UKIn the title compound, C24H22N4O2S, the dihedral angle between the triazole and thiophene rings is 4.83 (14)°. The dihedral angles between the triazole and tolyl rings and between the thiophene and phenyl rings are 48.42 (16) and 9.23 (13)°, respectively. An intramolecular N—H...O hydrogen bond closes an S(6) loop. In the crystal, molecules are stacked parallel to the a-axis direction with weak π–π interactions between adjacent thiophenyl and triazolyl groups within the stack [centroid–centroid separation = 3.9811 (16) Å].http://scripts.iucr.org/cgi-bin/paper?S2414314618004029crystal structure1,2,3-triazolethiophene
collection	DOAJ
language	English
format	Article
sources	DOAJ
author	Gamal A. El-Hiti Bakr F. Abdel-Wahab Rizk E. Khidre Mohamed S. Mostafa Amany S. Hegazy Benson M. Kariuki
spellingShingle	Gamal A. El-Hiti Bakr F. Abdel-Wahab Rizk E. Khidre Mohamed S. Mostafa Amany S. Hegazy Benson M. Kariuki 1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone IUCrData crystal structure 1,2,3-triazole thiophene
author_facet	Gamal A. El-Hiti Bakr F. Abdel-Wahab Rizk E. Khidre Mohamed S. Mostafa Amany S. Hegazy Benson M. Kariuki
author_sort	Gamal A. El-Hiti
title	1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone
title_short	1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone
title_full	1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone
title_fullStr	1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone
title_full_unstemmed	1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone
title_sort	1-{2-anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1h-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone
publisher	International Union of Crystallography
series	IUCrData
issn	2414-3146
publishDate	2018-03-01
description	In the title compound, C24H22N4O2S, the dihedral angle between the triazole and thiophene rings is 4.83 (14)°. The dihedral angles between the triazole and tolyl rings and between the thiophene and phenyl rings are 48.42 (16) and 9.23 (13)°, respectively. An intramolecular N—H...O hydrogen bond closes an S(6) loop. In the crystal, molecules are stacked parallel to the a-axis direction with weak π–π interactions between adjacent thiophenyl and triazolyl groups within the stack [centroid–centroid separation = 3.9811 (16) Å].
topic	crystal structure 1,2,3-triazole thiophene
url	http://scripts.iucr.org/cgi-bin/paper?S2414314618004029
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1-{2-Anilino-4-methyl-5-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]thiophen-3-yl}ethanone

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