Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples
Mixed iron-manganese oxide nanoparticles, synthesized by a simple procedure, were used to remove nickel ion from aqueous solutions. Nanostructures, prepared by using different weight percents of manganese, were characterized by transmission electron microscopy, selected area diffraction, X-ray diffr...
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doaj-c792e23002c04d3693790ecb6da0350f2020-11-25T00:15:26ZengHindawi LimitedJournal of Analytical Methods in Chemistry2090-88652090-88732017-01-01201710.1155/2017/94760659476065Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous SamplesAlessandro Buccolieri0Antonio Serra1Giuseppe Maruccio2Anna Grazia Monteduro3Sanosh Kunjalukkal Padmanabhan4Antonio Licciulli5Valentina Bonfrate6Luca Salvatore7Daniela Manno8Lucio Calcagnile9Gabriele Giancane10Department of Biological and Environmental Sciences and Technologies (DiSTeBA), Università del Salento, Via Per Arnesano, 73100 Lecce, ItalyDepartment of Mathematics and Physics “E. De Giorgi”, Università del Salento, Via Per Arnesano, 73100 Lecce, ItalyDepartment of Mathematics and Physics “E. De Giorgi”, Università del Salento, Via Per Arnesano, 73100 Lecce, ItalyIRCCS, National Institute of Gastroenterology “S. de Bellis”, Castellana Grotte, 70013 Bari, ItalyDepartment of Engineering for Innovation, Università del Salento, Via Monteroni, 73100 Lecce, ItalyDepartment of Engineering for Innovation, Università del Salento, Via Monteroni, 73100 Lecce, ItalyDepartment of Engineering for Innovation, Università del Salento, Via Monteroni, 73100 Lecce, ItalyDepartment of Engineering for Innovation, Università del Salento, Via Monteroni, 73100 Lecce, ItalyDepartment of Mathematics and Physics “E. De Giorgi”, Università del Salento, Via Per Arnesano, 73100 Lecce, ItalyDepartment of Mathematics and Physics “E. De Giorgi”, Università del Salento, Via Per Arnesano, 73100 Lecce, ItalyDepartment of Cultural Heritage, Università del Salento, Via D. Birago, 73100 Lecce, ItalyMixed iron-manganese oxide nanoparticles, synthesized by a simple procedure, were used to remove nickel ion from aqueous solutions. Nanostructures, prepared by using different weight percents of manganese, were characterized by transmission electron microscopy, selected area diffraction, X-ray diffraction, Raman spectroscopy, and vibrating sample magnetometry. Adsorption/desorption isotherm curves demonstrated that manganese inclusions enhance the specific surface area three times and the pores volume ten times. This feature was crucial to decontaminate both aqueous samples and food extracts from nickel ion. Efficient removal of Ni2+ was highlighted by the well-known dimethylglyoxime test and by ICP-MS analysis and the possibility of regenerating the nanostructure was obtained by a washing treatment in disodium ethylenediaminetetraacetate solution.http://dx.doi.org/10.1155/2017/9476065 |
collection |
DOAJ |
language |
English |
format |
Article |
sources |
DOAJ |
author |
Alessandro Buccolieri Antonio Serra Giuseppe Maruccio Anna Grazia Monteduro Sanosh Kunjalukkal Padmanabhan Antonio Licciulli Valentina Bonfrate Luca Salvatore Daniela Manno Lucio Calcagnile Gabriele Giancane |
spellingShingle |
Alessandro Buccolieri Antonio Serra Giuseppe Maruccio Anna Grazia Monteduro Sanosh Kunjalukkal Padmanabhan Antonio Licciulli Valentina Bonfrate Luca Salvatore Daniela Manno Lucio Calcagnile Gabriele Giancane Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples Journal of Analytical Methods in Chemistry |
author_facet |
Alessandro Buccolieri Antonio Serra Giuseppe Maruccio Anna Grazia Monteduro Sanosh Kunjalukkal Padmanabhan Antonio Licciulli Valentina Bonfrate Luca Salvatore Daniela Manno Lucio Calcagnile Gabriele Giancane |
author_sort |
Alessandro Buccolieri |
title |
Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples |
title_short |
Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples |
title_full |
Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples |
title_fullStr |
Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples |
title_full_unstemmed |
Synthesis and Characterization of Mixed Iron-Manganese Oxide Nanoparticles and Their Application for Efficient Nickel Ion Removal from Aqueous Samples |
title_sort |
synthesis and characterization of mixed iron-manganese oxide nanoparticles and their application for efficient nickel ion removal from aqueous samples |
publisher |
Hindawi Limited |
series |
Journal of Analytical Methods in Chemistry |
issn |
2090-8865 2090-8873 |
publishDate |
2017-01-01 |
description |
Mixed iron-manganese oxide nanoparticles, synthesized by a simple procedure, were used to remove nickel ion from aqueous solutions. Nanostructures, prepared by using different weight percents of manganese, were characterized by transmission electron microscopy, selected area diffraction, X-ray diffraction, Raman spectroscopy, and vibrating sample magnetometry. Adsorption/desorption isotherm curves demonstrated that manganese inclusions enhance the specific surface area three times and the pores volume ten times. This feature was crucial to decontaminate both aqueous samples and food extracts from nickel ion. Efficient removal of Ni2+ was highlighted by the well-known dimethylglyoxime test and by ICP-MS analysis and the possibility of regenerating the nanostructure was obtained by a washing treatment in disodium ethylenediaminetetraacetate solution. |
url |
http://dx.doi.org/10.1155/2017/9476065 |
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