Synthesis And characterization of 1-[(N-tetra-O-acetyl-β-D-glucopyranosyl)thioamido]-5-substituted-2-imino-4-thiobiuret
<div>A novel synthesis of 1-[(N-tetra-O-acetyl-ß-D-glucopyranosyl)thioamido]-5-substituted-2-imino-4-thiobiurets (3) was carried out by the reaction of tetra-O-acetyl-ß-D-glucopyranosylisothiocynate (1) with 1-substituted-3-formamidino-thiocarbamides (2) in acetone-ethanol (1:1) medium. The pr...
| Main Authors: | , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
Universidade Federal de Mato Grosso do Sul
2011-08-01
|
| Series: | Orbital: The Electronic Journal of Chemistry |
| Subjects: | |
| Online Access: | http://orbital.ufms.br/index.php/Chemistry/article/view/201 |
| Summary: | <div>A novel synthesis of 1-[(N-tetra-O-acetyl-ß-D-glucopyranosyl)thioamido]-5-substituted-2-imino-4-thiobiurets (3) was carried out by the reaction of tetra-O-acetyl-ß-D-glucopyranosylisothiocynate (1) with 1-substituted-3-formamidino-thiocarbamides (2) in acetone-ethanol (1:1) medium. The prepared compounds have been purified and their structures were established on the basis of their gasometric analysis, chemical characteristics, elemental analysis, 1H-spectra, as well as by their IR and MS spectra.</div> |
|---|---|
| ISSN: | 1984-6428 |